meptazinol para-amino-meta-methoxybenzoic acid carbamate hydrochloride

Base Information

Chemical Name:meptazinol para-amino-meta-methoxybenzoic acid carbamate hydrochloride
CAS No.:1314003-20-7
Molecular Formula:C₂₄H₃₀N₂O₅*ClH
Molecular Weight:462.974
Hs Code.:

Synonyms:meptazinol para-amino-meta-methoxybenzoic acid carbamate hydrochloride

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Chemical Property of meptazinol para-amino-meta-methoxybenzoic acid carbamate hydrochloride

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Technology Process of meptazinol para-amino-meta-methoxybenzoic acid carbamate hydrochloride

There total 5 articles about meptazinol para-amino-meta-methoxybenzoic acid carbamate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1314003-68-3
meptazinol para-amino-meta-methoxybenzoic acid carbamate

: 1314003-20-7
meptazinol para-amino-meta-methoxybenzoic acid carbamate hydrochloride

Guidance literature:: With hydrogenchloride; In tetrahydrofuran; diethyl ether;

Reference yield:

: 5081-36-7
3-methoxy-4-nitrobenzoic acid

: 1314003-20-7
meptazinol para-amino-meta-methoxybenzoic acid carbamate hydrochloride

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 21 h / 80 °C / Inert atmosphere

2.1: tin(II) chloride dihdyrate / ethanol / 1.25 h / 80 °C / Inert atmosphere

3.1: triethylamine / toluene; tetrahydrofuran / 0.76 h / -76 - -70 °C / Inert atmosphere

3.2: 1 h / -76 - 20 °C / Inert atmosphere

4.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 18 h / 0 - 15 °C / Inert atmosphere

5.1: hydrogenchloride / diethyl ether; tetrahydrofuran

With hydrogenchloride; tin(II) chloride dihdyrate; hydrogen; potassium carbonate; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; diethyl ether; ethanol; N,N-dimethyl-formamide; toluene; 3.1: Schotten-Baumann Reaction;

Reference yield:

: 190330-56-4
benzyl 4-amino-3-methoxybenzoate

: 1314003-20-7
meptazinol para-amino-meta-methoxybenzoic acid carbamate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / toluene; tetrahydrofuran / 0.76 h / -76 - -70 °C / Inert atmosphere

1.2: 1 h / -76 - 20 °C / Inert atmosphere

2.1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran / 18 h / 0 - 15 °C / Inert atmosphere

3.1: hydrogenchloride / diethyl ether; tetrahydrofuran

With hydrogenchloride; hydrogen; triethylamine; palladium 10% on activated carbon; In tetrahydrofuran; diethyl ether; toluene; 1.1: Schotten-Baumann Reaction;