(S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(5-(6-methoxynaphthalen-2-yl)-1H-imidazol-2-yl)heptanoate

Base Information

Chemical Name:(S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(5-(6-methoxynaphthalen-2-yl)-1H-imidazol-2-yl)heptanoate
CAS No.:1609191-11-8
Molecular Formula:C₃₃H₃₉N₃O₅
Molecular Weight:557.69
Hs Code.:

Synonyms:(S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(5-(6-methoxynaphthalen-2-yl)-1H-imidazol-2-yl)heptanoate

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Chemical Property of (S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(5-(6-methoxynaphthalen-2-yl)-1H-imidazol-2-yl)heptanoate

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Technology Process of (S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(5-(6-methoxynaphthalen-2-yl)-1H-imidazol-2-yl)heptanoate

There total 6 articles about (S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(5-(6-methoxynaphthalen-2-yl)-1H-imidazol-2-yl)heptanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1609191-05-0
C₂₂H₃₀IN₃O₄

: 156641-98-4
(6-methoxy-2-naphthalene)boronic acid

: 1609191-11-8
(S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(5-(6-methoxynaphthalen-2-yl)-1H-imidazol-2-yl)heptanoate

Guidance literature:: With palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium carbonate; In 1,2-dimethoxyethane; water; at 110 ℃; for 0.666667h;

Reference yield:

: 1609191-04-9
⁽⁵⁾-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(1H-imidazol-2-yl)heptanoate

: 1609191-11-8
(S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(5-(6-methoxynaphthalen-2-yl)-1H-imidazol-2-yl)heptanoate

Guidance literature:: Multi-step reaction with 3 steps

1: N-iodo-succinimide / acetonitrile / 2 h / -10 °C

2: sodium sulfite; tetrabutylammonium dihydrogen phosphate / water; 1,4-dioxane / 0.5 h / 160 °C / Microwave irradiation

3: palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium carbonate / water; 1,2-dimethoxyethane / 0.67 h / 110 °C

With N-iodo-succinimide; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium carbonate; tetrabutylammonium dihydrogen phosphate; sodium sulfite; In 1,4-dioxane; 1,2-dimethoxyethane; water; acetonitrile;

Reference yield:

: 1609191-03-8
(S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-8-oxooctanoate

: 1609191-11-8
(S)-tert-butyl 7-(((benzyloxy)carbonyl)amino)-7-(5-(6-methoxynaphthalen-2-yl)-1H-imidazol-2-yl)heptanoate

Guidance literature:: Multi-step reaction with 4 steps

1: ammonia / methanol / 72 h / 20 °C / Sealed tube

2: N-iodo-succinimide / acetonitrile / 2 h / -10 °C

3: sodium sulfite; tetrabutylammonium dihydrogen phosphate / water; 1,4-dioxane / 0.5 h / 160 °C / Microwave irradiation

4: palladium bis[bis(diphenylphosphino)ferrocene] dichloride; potassium carbonate / water; 1,2-dimethoxyethane / 0.67 h / 110 °C

With N-iodo-succinimide; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; ammonia; potassium carbonate; tetrabutylammonium dihydrogen phosphate; sodium sulfite; In 1,4-dioxane; methanol; 1,2-dimethoxyethane; water; acetonitrile;