2-chloro-5-(Boc-amino)benzyl mesylate

Base Information

Chemical Name:2-chloro-5-(Boc-amino)benzyl mesylate
CAS No.:200214-49-9
Molecular Formula:C₁₃H₁₈ClNO₅S
Molecular Weight:335.809
Hs Code.:

Synonyms:2-chloro-5-(Boc-amino)benzyl mesylate

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Chemical Property of 2-chloro-5-(Boc-amino)benzyl mesylate

Chemical Property:

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Technology Process of 2-chloro-5-(Boc-amino)benzyl mesylate

There total 3 articles about 2-chloro-5-(Boc-amino)benzyl mesylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 200214-48-8
tert-butyl N-[4-chloro-3-(hydroxymethyl)phenyl]carbamate

: 124-63-0
methanesulfonyl chloride

: 200214-49-9
2-chloro-5-(Boc-amino)benzyl mesylate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2006.11.078

Reference yield:

: 80866-80-4
2-chloro-5-nitrobenzyl alcohol

: 200214-49-9
2-chloro-5-(Boc-amino)benzyl mesylate

Guidance literature:: Multi-step reaction with 3 steps

1: Fe; HCl / ethanol

2: DIEA / CH₂Cl₂

With hydrogenchloride; iron; N-ethyl-N,N-diisopropylamine; In ethanol; dichloromethane;
DOI:10.1016/j.bmcl.2006.11.078

Reference yield:

: 89951-56-4
4-chloro-5-hydroxymethyl aniline

: 200214-49-9
2-chloro-5-(Boc-amino)benzyl mesylate

Guidance literature:: Multi-step reaction with 2 steps

1: DIEA / CH₂Cl₂

With N-ethyl-N,N-diisopropylamine; In dichloromethane;
DOI:10.1016/j.bmcl.2006.11.078