5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Base Information

Chemical Name:5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin
CAS No.:129618-98-0
Molecular Formula:C₄₇H₅₂N₄O₃
Molecular Weight:720.955
Hs Code.:

Synonyms:5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

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Chemical Property of 5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

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Technology Process of 5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

There total 4 articles about 5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4949-58-0
2-(ethyloxycarbonyl)-3-ethyl-4-methylpyrrole

: 129618-98-0
5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 75 percent / HCl / ethanol / 8 h / Heating

2: 1.) NaOH / 1.) aq. EtOH, reflux, 2 h, 2.) ethanediol, 185 deg C, 30 min

3: 1.) aq. HClO₄, 2.) o-chloranil / 1.) THF, MeOH, 25 deg C, 12 h, 2.) THF, MeOH, 3 h

With hydrogenchloride; sodium hydroxide; perchloric acid; o-tetrachloroquinone; In ethanol;
DOI:10.1021/ja00064a025

Reference yield:

: 129618-96-8
bis(5-(ethoxycarbonyl)-4-ethyl-3-methyl-2-pyrryl)(4-(hydroxymethyl)phenyl)methane

: 129618-98-0
5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaOH / 1.) aq. EtOH, reflux, 2 h, 2.) ethanediol, 185 deg C, 30 min

2: 1.) aq. HClO₄, 2.) o-chloranil / 1.) THF, MeOH, 25 deg C, 12 h, 2.) THF, MeOH, 3 h

With sodium hydroxide; perchloric acid; o-tetrachloroquinone;
DOI:10.1021/ja00064a025

Reference yield:

: 129618-97-9
bis(4-ethyl-3-methyl-2-pyrryl)(4-(hydroxymethyl)phenyl)methane

: 108895-17-6
bis(4-ethyl-5-formyl-3-methyl-2-pyrryl)(2,5-dimethoxyphenyl)methane

: 129618-98-0
5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Guidance literature:: With perchloric acid; o-tetrachloroquinone; Yield given. Multistep reaction; 1.) THF, MeOH, 25 deg C, 12 h, 2.) THF, MeOH, 3 h;
DOI:10.1021/ja00064a025