5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Base Information

Chemical Name:5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin
CAS No.:129618-99-1
Molecular Formula:C₄₇H₅₀N₄O₃
Molecular Weight:718.939
Hs Code.:

Synonyms:5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Suppliers and Price of 5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

There total 6 articles about 5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 129618-98-0
5-(2',5'-dimethoxyphenyl)-15-(4''-(hydroxymethyl)phenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

: 129618-99-1
5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Guidance literature:: With dipyridinium dichromate; In dichloromethane;
DOI:10.1021/ja00064a025

Reference yield:

: 4949-58-0
2-(ethyloxycarbonyl)-3-ethyl-4-methylpyrrole

: 129618-99-1
5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Guidance literature:: Multi-step reaction with 4 steps

1: 75 percent / HCl / ethanol / 8 h / Heating

2: 1.) NaOH / 1.) aq. EtOH, reflux, 2 h, 2.) ethanediol, 185 deg C, 30 min

3: 1.) aq. HClO₄, 2.) o-chloranil / 1.) THF, MeOH, 25 deg C, 12 h, 2.) THF, MeOH, 3 h

4: 88 percent / pyridinium dichromate (PDC) / CH₂Cl₂

With hydrogenchloride; sodium hydroxide; dipyridinium dichromate; perchloric acid; o-tetrachloroquinone; In ethanol; dichloromethane;
DOI:10.1021/ja00064a025

Reference yield:

: 129618-96-8
bis(5-(ethoxycarbonyl)-4-ethyl-3-methyl-2-pyrryl)(4-(hydroxymethyl)phenyl)methane

: 129618-99-1
5-(4'-formylphenyl)-15-(2'',5''-dimethoxyphenyl)-2,8,12,18-tetraethyl-3,7,13,17-tetramethylporphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) NaOH / 1.) aq. EtOH, reflux, 2 h, 2.) ethanediol, 185 deg C, 30 min

2: 1.) aq. HClO₄, 2.) o-chloranil / 1.) THF, MeOH, 25 deg C, 12 h, 2.) THF, MeOH, 3 h

3: 88 percent / pyridinium dichromate (PDC) / CH₂Cl₂

With sodium hydroxide; dipyridinium dichromate; perchloric acid; o-tetrachloroquinone; In dichloromethane;
DOI:10.1021/ja00064a025