methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Base Information

Chemical Name:methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside
CAS No.:155630-81-2
Molecular Formula:C₄₃H₄₉NO₁₄
Molecular Weight:803.86
Hs Code.:

Synonyms:methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Suppliers and Price of methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

There total 3 articles about methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 155630-80-1
methyl 6-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronate)-α-D-glucopyranoside

: 155630-81-2
methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Guidance literature:: With sodium hydroxide; In methanol; dichloromethane; at 20 ℃; for 2h;
DOI:10.1016/S0008-6215(00)90986-8

Reference yield:

: 4-methoxyphenyl 2,2,2-trichloroacetimidate

: 155630-81-2
methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / trifluoromethanesulphonic acid / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

2: 92 percent / 4M aq. NaOH / CH₂Cl₂; methanol / 2 h / 20 °C

With sodium hydroxide; trifluorormethanesulfonic acid; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/S0008-6215(00)90986-8

Reference yield:

: 114869-97-5
methyl 6-O-acetyl-3-O-benzyl-2-benzyloxycarbonylamino-2-deoxy-4-O-(methyl 2-O-acetyl-3-O-benzyl-α-L-idopyranosyluronate)-α-D-glucopyranoside

: 155630-81-2
methyl 3-O-benzyl-4-O-(3-O-benzyl-4-O-p-methoxybenzyl-α-L-idopyranosyluronic acid)-2-benzyloxycarbonylamino-2-deoxy-α-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / trifluoromethanesulphonic acid / CH₂Cl₂; diethyl ether / 0.5 h / 20 °C

2: 92 percent / 4M aq. NaOH / CH₂Cl₂; methanol / 2 h / 20 °C

With sodium hydroxide; trifluorormethanesulfonic acid; In methanol; diethyl ether; dichloromethane;
DOI:10.1016/S0008-6215(00)90986-8