N-(4-((4-amino-2,3-dichlorophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

Base Information

Chemical Name:N-(4-((4-amino-2,3-dichlorophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide
CAS No.:1337932-33-8
Molecular Formula:C₁₅H₁₅Cl₂N₃O₂S
Molecular Weight:372.275
Hs Code.:

Synonyms:N-(4-((4-amino-2,3-dichlorophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

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Chemical Property of N-(4-((4-amino-2,3-dichlorophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

Chemical Property:

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Technology Process of N-(4-((4-amino-2,3-dichlorophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

There total 4 articles about N-(4-((4-amino-2,3-dichlorophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1337932-32-7
N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

: 1337932-33-8
N-(4-((4-amino-2,3-dichlorophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

Guidance literature:: N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide; With iron; acetic acid; at 50 ℃; for 1h;

With potassium carbonate; In ethyl acetate; at 20 ℃;

Reference yield:

: 864461-13-2
4-(bromomethyl)pyridin-2-amine hydrobromide

: 1337932-33-8
N-(4-((4-amino-2,3-dichlorophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogen sulfide / N,N-dimethyl-formamide / 1 h / Inert atmosphere

1.2: 1 h / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane; tetrahydrofuran / 1.17 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h

3.1: acetic acid; iron / 1 h / 50 °C

3.2: 20 °C

With sodium hydrogen sulfide; iron; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 36556-51-1
2,3-dichloro-1-fluoro-4-nitrobenzene

: 1337932-33-8
N-(4-((4-amino-2,3-dichlorophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydrogen sulfide / N,N-dimethyl-formamide / 1 h / Inert atmosphere

1.2: 1 h / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane; tetrahydrofuran / 1.17 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h

3.1: acetic acid; iron / 1 h / 50 °C

3.2: 20 °C

With sodium hydrogen sulfide; iron; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;