N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

Base Information

Chemical Name:N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide
CAS No.:1337932-32-7
Molecular Formula:C₁₅H₁₃Cl₂N₃O₄S
Molecular Weight:402.258
Hs Code.:

Synonyms:N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

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Chemical Property of N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

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Technology Process of N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

There total 3 articles about N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 38870-89-2
Methoxyacetyl chloride

: 1337932-31-6
4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-amine

: 1337932-32-7
N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

Guidance literature:: Methoxyacetyl chloride; 4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-amine; With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; at 0 - 20 ℃; for 1.16667h; Inert atmosphere;

With ammonia; In tetrahydrofuran; methanol; dichloromethane; for 0.5h;

Reference yield:

: 864461-13-2
4-(bromomethyl)pyridin-2-amine hydrobromide

: 1337932-32-7
N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogen sulfide / N,N-dimethyl-formamide / 1 h / Inert atmosphere

1.2: 1 h / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane; tetrahydrofuran / 1.17 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h

With sodium hydrogen sulfide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 36556-51-1
2,3-dichloro-1-fluoro-4-nitrobenzene

: 1337932-32-7
N-(4-((2,3-dichloro-4-nitrophenylthio)methyl)pyridin-2-yl)-2-methoxyacetamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydrogen sulfide / N,N-dimethyl-formamide / 1 h / Inert atmosphere

1.2: 1 h / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane; tetrahydrofuran / 1.17 h / 0 - 20 °C / Inert atmosphere

2.2: 0.5 h

With sodium hydrogen sulfide; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;