12-(4-nitrophenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one

Base Information

• Chemical Name: 12-(4-nitrophenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one
• CAS No.: 114382-97-7
• Molecular Formula: C₂₃H₁₇NO₄
• Molecular Weight: 371.392
• Mol file: 114382-97-7.mol

Synonyms:12-(4-nitrophenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one

Chemical Property of 12-(4-nitrophenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 12-(4-nitrophenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one

There total 2 articles about 12-(4-nitrophenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

1,3-cylohexanedione (504-02-9) + 4-nitrobenzaldehdye (555-16-8) + β-naphthol (135-19-3) → 12-(4-nitrophenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one (114382-97-7)

Guidance literature:

With chitosan modified with Fe₃O₄ and silver nanoparticles; In water; at 80 ℃; for 0.416667h; Green chemistry;

DOI:10.1016/j.molcata.2014.06.005

Reference yield:

→ 12-(4-nitrophenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one (114382-97-7)

Guidance literature:

β-Naphthol, Dihydro-resorcin, p-Nitro-benzaldehyd, sd. Eg., 1 h;

Reference yield: 85.0%

12-(4-nitrophenyl)-8,9,10,12-tetrahydro-11H-benzo[a]xanthen-11-one (114382-97-7) → C23H17NO3S (1416451-37-0)

Guidance literature:

With Lawessons reagent; In toluene; for 1.5h; Reflux;

DOI:10.1016/j.ejmech.2012.10.025

upstream raw materials:

1,3-cylohexanedione

4-nitrobenzaldehdye

β-naphthol

Downstream raw materials:

C₂₃H₁₇NO₃S