2,3-Diphenylphenanthro[9,10-b]furan

Base Information

Chemical Name:2,3-Diphenylphenanthro[9,10-b]furan
CAS No.:22725-49-1
Molecular Formula:C₂₈H₁₈O
Molecular Weight:370.45
Hs Code.:
NSC Number:136094
DSSTox Substance ID:DTXSID10300341
Nikkaji Number:J3.056.057D
Wikidata:Q82043320

Synonyms:2,3-diphenylphenanthro[9,10-b]furan;22725-49-1;NSC136094;SCHEMBL2620727;DTXSID10300341;NSC-136094

Suppliers and Price of 2,3-Diphenylphenanthro[9,10-b]furan

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2,3-Diphenylphenanthro[9,10-b]furan

Chemical Property:

Vapor Pressure:5.04E-12mmHg at 25°C
XLogP3:7.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:370.135765193
Heavy Atom Count:29
Complexity:545

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=C(OC3=C2C4=CC=CC=C4C5=CC=CC=C53)C6=CC=CC=C6

Technology Process of 2,3-Diphenylphenanthro[9,10-b]furan

There total 3 articles about 2,3-Diphenylphenanthro[9,10-b]furan which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 2,3-dihydro-2,3-diphenylphenanthro[9,10-b]furan

: 22725-49-1
2,3-diphenylphenanthro[9,10-b]furan

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In toluene; at 70 ℃; for 3h;
DOI:10.1246/bcsj.20160093

Reference yield:

: 1100-88-5
benzyltriphenylphosphonium chloride

: 22725-49-1
2,3-diphenylphenanthro[9,10-b]furan

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium tert-butylate / dimethyl sulfoxide / 0.03 h / 20 °C

1.2: 0.5 h / 20 °C

2.1: 2,3-dicyano-5,6-dichloro-p-benzoquinone / toluene / 3 h / 70 °C

With potassium tert-butylate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dimethyl sulfoxide; toluene;
DOI:10.1246/bcsj.20160093