1-O-(α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol

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Chemical Name:1-O-(α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol
CAS No.:1204401-08-0
Molecular Formula:C₄₇H₇₆FNO₁₀
Molecular Weight:834.12
Hs Code.:

Synonyms:1-O-(α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol

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Chemical Property of 1-O-(α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol

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Technology Process of 1-O-(α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol

There total 10 articles about 1-O-(α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 3,4-di-O-benzyl-1-O-(2,3-di-O-benzyl-4,6-O-benzylidene-α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol

: 1204401-08-0
1-O-(α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol

Guidance literature:: With hydrogen; palladium(II) hydroxide; In methanol; dichloromethane; at 20 ℃; for 10h; under 3750.38 Torr;

Reference yield:

: C₆₈H₉₄FNO₁₀

: 1204401-08-0
1-O-(α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol

Guidance literature:: With 20% palladium hydroxide on charcoal; hydrogen; acetic acid; In methanol; chloroform; at 20 ℃; for 24h;
DOI:10.1128/AAC.00368-10

Reference yield:

: 1204527-69-4
C₅₀H₇₁N₃O₉

: 1204401-08-0
1-O-(α-D-galactopyranosyl)-2-(11-(4-(4-fluorophenoxy)phenyl)undecanoyl)amino-D-ribo-octadecane-1,3,4-triol

Guidance literature:: Multi-step reaction with 4 steps

1.1: pyridine; triphenylphosphine / water / 16 h / 45 °C

2.1: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane / 16 h / 20 °C

3.1: methanol; sodium methylate / dichloromethane / 20 °C

3.2: 16 h / 70 °C

4.1: 20% palladium hydroxide on charcoal; hydrogen; acetic acid / methanol; chloroform / 24 h / 20 °C

With pyridine; methanol; 20% palladium hydroxide on charcoal; hydrogen; sodium methylate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; triphenylphosphine; In methanol; dichloromethane; chloroform; water; 1.1: Staudinger reaction;
DOI:10.1128/AAC.00368-10