C₁₈H₂₆FNO₄

Base Information

Chemical Name:C₁₈H₂₆FNO₄
CAS No.:1272598-52-3
Molecular Formula:C₁₈H₂₆FNO₄
Molecular Weight:339.407
Hs Code.:

C<sub>18</sub>H<sub>26</sub>FNO<sub>4</sub>

Synonyms:C₁₈H₂₆FNO₄

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Chemical Property of C₁₈H₂₆FNO₄

Chemical Property:

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Technology Process of C₁₈H₂₆FNO₄

There total 4 articles about C₁₈H₂₆FNO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 1272598-50-1
C₁₈H₂₇NO₅

: 1272598-52-3
C₁₈H₂₆FNO₄

Guidance literature:: With (bis-(2-methoxyethyl)amino)sulfur trufluoride; In dichloromethane; at -78 - 20 ℃;
DOI:10.1016/j.bmcl.2010.12.078

Reference yield:

: 1272599-25-3
C₁₈H₂₇NO₅

: 1272598-52-3
C₁₈H₂₆FNO₄

Guidance literature:: Multi-step reaction with 2 steps

1.1: formic acid; di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / Reflux

1.2: 20 °C

2.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / -78 - 20 °C

With formic acid; di-isopropyl azodicarboxylate; triphenylphosphine; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; dichloromethane; 1.1: Mitsunobu reaction / 1.2: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2010.12.078

Reference yield:

: 184046-78-4
(2S,3S)-1-tert-butyl-2-methyl 3-hydroxypyrrolidine-1,2-dicarboxylate

: 1272598-52-3
C₁₈H₂₆FNO₄

Guidance literature:: Multi-step reaction with 4 steps

1.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C

2.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 0 - 20 °C

3.1: formic acid; di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / Reflux

3.2: 20 °C

4.1: (bis-(2-methoxyethyl)amino)sulfur trufluoride / dichloromethane / -78 - 20 °C

With lithium borohydride; formic acid; di-isopropyl azodicarboxylate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; (bis-(2-methoxyethyl)amino)sulfur trufluoride; In tetrahydrofuran; dichloromethane; 3.1: Mitsunobu reaction / 3.2: Mitsunobu reaction;
DOI:10.1016/j.bmcl.2010.12.078