[(3,4-Dimethyl-phenyl)-(3-mercapto-2-methyl-propionyl)-amino]-acetic acid

Base Information

Chemical Name:[(3,4-Dimethyl-phenyl)-(3-mercapto-2-methyl-propionyl)-amino]-acetic acid
CAS No.:86323-99-1
Molecular Formula:C₁₄H₁₉NO₃S
Molecular Weight:281.376
Hs Code.:

Synonyms:[(3,4-Dimethyl-phenyl)-(3-mercapto-2-methyl-propionyl)-amino]-acetic acid

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Chemical Property of [(3,4-Dimethyl-phenyl)-(3-mercapto-2-methyl-propionyl)-amino]-acetic acid

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Technology Process of [(3,4-Dimethyl-phenyl)-(3-mercapto-2-methyl-propionyl)-amino]-acetic acid

There total 3 articles about [(3,4-Dimethyl-phenyl)-(3-mercapto-2-methyl-propionyl)-amino]-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 95-64-7
4-amino-o-xylene

: 86323-99-1
[(3,4-Dimethyl-phenyl)-(3-mercapto-2-methyl-propionyl)-amino]-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: sodium acetate trihydrate / 110 °C

2: K₂CO₃ / CH₂Cl₂ / 2 h / Ambient temperature

3: 2.08 N aq. KOH / methanol / 2 h / Ambient temperature

With potassium hydroxide; sodium acetate; potassium carbonate; In methanol; dichloromethane;
DOI:10.1021/jm00363a011

Reference yield:

: [(3-Acetylsulfanyl-2-methyl-propionyl)-(3,4-dimethyl-phenyl)-amino]-acetic acid ethyl ester

: 86323-99-1
[(3,4-Dimethyl-phenyl)-(3-mercapto-2-methyl-propionyl)-amino]-acetic acid

Guidance literature:: With potassium hydroxide; In methanol; for 2h; Ambient temperature;
DOI:10.1021/jm00363a011

Reference yield:

: 2371-26-8
N-(3,4-dimethylphenyl)glycine ethyl ester

: 86323-99-1
[(3,4-Dimethyl-phenyl)-(3-mercapto-2-methyl-propionyl)-amino]-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: K₂CO₃ / CH₂Cl₂ / 2 h / Ambient temperature

2: 2.08 N aq. KOH / methanol / 2 h / Ambient temperature

With potassium hydroxide; potassium carbonate; In methanol; dichloromethane;
DOI:10.1021/jm00363a011