ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol

Base Information

Chemical Name:ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol
CAS No.:118098-96-7
Molecular Formula:C₄₀H₅₈O₁₅S₂
Molecular Weight:843.024
Hs Code.:

Synonyms:ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol

Suppliers and Price of ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol

There total 4 articles about ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 118069-29-7
13-(benzyloxymethyl)-3,6,9,12,15,18,21,24-octaoxa-1,26-hexacosanediol

: 118098-96-7
ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol

Guidance literature:: With p-toluenesulfonyl chloride; In pyridine; at 0 ℃; overnight;
DOI:10.1002/recl.19881070209

Reference yield:

: 5197-66-0
2-(2-(2-(2-chloroethoxy)ethoxy)ethoxy)ethanol

: 118098-96-7
ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent / HCl / 1 h / Ambient temperature

2: 32 percent / Li, LiBr / 2-methyl-propan-2-ol / 360 h / Heating

3: 100 percent / HCl / CH₂Cl₂; methanol / 3 h / Ambient temperature

4: 98 percent / p-toluenesulfonyl chloride / pyridine / 0 °C / overnight

With hydrogenchloride; lithium; p-toluenesulfonyl chloride; lithium bromide; In pyridine; methanol; dichloromethane; tert-butyl alcohol;
DOI:10.1002/recl.19881070209

Reference yield:

: 90213-14-2
tetrahydropyranyl ether of 11-chloro-3,6,9-trioxa-1-undecanol

: 118098-96-7
ditosylate of 13-(benzyloxymethyl)-3,6,9,12,15,18,24-octaoxa-1,26-hexacosanediol

Guidance literature:: Multi-step reaction with 3 steps

1: 32 percent / Li, LiBr / 2-methyl-propan-2-ol / 360 h / Heating

2: 100 percent / HCl / CH₂Cl₂; methanol / 3 h / Ambient temperature

3: 98 percent / p-toluenesulfonyl chloride / pyridine / 0 °C / overnight

With hydrogenchloride; lithium; p-toluenesulfonyl chloride; lithium bromide; In pyridine; methanol; dichloromethane; tert-butyl alcohol;
DOI:10.1002/recl.19881070209