2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetic acid

Base Information

Chemical Name:2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetic acid
CAS No.:1415926-48-5
Molecular Formula:C₂₃H₃₆O₄
Molecular Weight:376.536
Hs Code.:

Synonyms:2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetic acid

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Technology Process of 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetic acid

There total 15 articles about 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1415704-73-2
methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate

: 1415926-48-5
2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetic acid

Guidance literature:: With lithium hydroxide monohydrate; dihydrogen peroxide; In tetrahydrofuran; water; at 20 ℃; for 24h;
DOI:10.1016/j.tet.2012.10.022

Reference yield:

: C₂₂H₃₂O₄

: 1415926-48-5
2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetic acid

Guidance literature:: Multi-step reaction with 6 steps

1.1: ethyl acetate; diethyl ether

2.1: titanium(IV) dichlorodiisopropylate / tetrahydrofuran / 0.25 h / 0 - 15 °C

3.1: bis(2,2,6,6-tetramethylheptane-3,5-dione)cobalt(II); oxygen / 1,2-dichloro-ethane / 2 h / 20 °C / 760.05 Torr

4.1: potassium carbonate / methanol / 5 h / 0 °C

5.1: pyridine / dichloromethane / 5 h / 0 - 20 °C

5.2: 1 h / 80 °C

6.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 24 h / 20 °C

With pyridine; titanium(IV) dichlorodiisopropylate; lithium hydroxide monohydrate; bis(2,2,6,6-tetramethylheptane-3,5-dione)cobalt(II); dihydrogen peroxide; oxygen; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; 5.1: |Barton-McCombie Deoxygenation / 5.2: |Barton-McCombie Deoxygenation;
DOI:10.1016/j.tet.2012.10.022

Reference yield:

: C₂₂H₃₄O₄

: 1415926-48-5
2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetic acid

Guidance literature:: Multi-step reaction with 7 steps

1.1: ruthenium trichloride; potassium carbonate; sodium periodate / water / 20 °C

2.1: ethyl acetate; diethyl ether

3.1: titanium(IV) dichlorodiisopropylate / tetrahydrofuran / 0.25 h / 0 - 15 °C

4.1: bis(2,2,6,6-tetramethylheptane-3,5-dione)cobalt(II); oxygen / 1,2-dichloro-ethane / 2 h / 20 °C / 760.05 Torr

5.1: potassium carbonate / methanol / 5 h / 0 °C

6.1: pyridine / dichloromethane / 5 h / 0 - 20 °C

6.2: 1 h / 80 °C

7.1: dihydrogen peroxide; lithium hydroxide monohydrate / tetrahydrofuran; water / 24 h / 20 °C

With pyridine; ruthenium trichloride; sodium periodate; titanium(IV) dichlorodiisopropylate; lithium hydroxide monohydrate; bis(2,2,6,6-tetramethylheptane-3,5-dione)cobalt(II); dihydrogen peroxide; oxygen; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; water; ethyl acetate; 1,2-dichloro-ethane; 6.1: |Barton-McCombie Deoxygenation / 6.2: |Barton-McCombie Deoxygenation;
DOI:10.1016/j.tet.2012.10.022