methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate

Base Information

Chemical Name:methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate
CAS No.:1415704-73-2
Molecular Formula:C₂₄H₃₈O₄
Molecular Weight:390.563
Hs Code.:

Synonyms:methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate

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Technology Process of methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate

There total 15 articles about methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)-2-((phenoxythiocarbonyl)oxy)acetate

: 1415704-73-2
methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate

Guidance literature:: DOI:10.1016/j.tet.2012.10.022

Reference yield:

: methyl (1R)-2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)-2-hydroxy acetate

: 1005-56-7
phenylcarbonochloridothioate

: 1415704-73-2
methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate

Guidance literature:: methyl (1R)-2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)-2-hydroxy acetate; phenylcarbonochloridothioate; With pyridine; In dichloromethane; at 0 - 20 ℃; for 5h;

With 2,2'-azobis(isobutyronitrile); tri-n-butyl-tin hydride; In toluene; at 80 ℃; for 1h;
DOI:10.1016/j.tet.2012.10.022

Reference yield:

: C₂₂H₃₂O₄

: 1415704-73-2
methyl 2-((3R,5R)-3,5-dimethyl-5-(10-phenyldecyl)-1,2-dioxolan-3-yl)acetate

Guidance literature:: Multi-step reaction with 5 steps

1.1: ethyl acetate; diethyl ether

2.1: titanium(IV) dichlorodiisopropylate / tetrahydrofuran / 0.25 h / 0 - 15 °C

3.1: bis(2,2,6,6-tetramethylheptane-3,5-dione)cobalt(II); oxygen / 1,2-dichloro-ethane / 2 h / 20 °C / 760.05 Torr

4.1: potassium carbonate / methanol / 5 h / 0 °C

5.1: pyridine / dichloromethane / 5 h / 0 - 20 °C

5.2: 1 h / 80 °C

With pyridine; titanium(IV) dichlorodiisopropylate; bis(2,2,6,6-tetramethylheptane-3,5-dione)cobalt(II); oxygen; potassium carbonate; In tetrahydrofuran; methanol; diethyl ether; dichloromethane; ethyl acetate; 1,2-dichloro-ethane; 5.1: |Barton-McCombie Deoxygenation / 5.2: |Barton-McCombie Deoxygenation;
DOI:10.1016/j.tet.2012.10.022