C₃₇H₄₉BrN₂O₁₀

Base Information

Chemical Name:C₃₇H₄₉BrN₂O₁₀
CAS No.:147363-14-2
Molecular Formula:C₃₇H₄₉BrN₂O₁₀
Molecular Weight:761.707
Hs Code.:

C<sub>37</sub>H<sub>49</sub>BrN<sub>2</sub>O<sub>10</sub>

Synonyms:C₃₇H₄₉BrN₂O₁₀

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Chemical Property of C₃₇H₄₉BrN₂O₁₀

Chemical Property:

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Technology Process of C₃₇H₄₉BrN₂O₁₀

There total 6 articles about C₃₇H₄₉BrN₂O₁₀ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 147363-14-2
C₃₇H₄₉BrN₂O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: i-Pr₂NEt / dimethylformamide / 8 h

2: potassium carbonate, n-Bu₄NI / dimethylformamide / 16 h

3: liquid NH₃ / methanol / 48 h / Ambient temperature

4: 90 percent / i-Pr₂NEt, DMAP, / CH₂Cl₂ / 2 h / Ambient temperature

5: 1.) NaN(TMS)2 / 2.) n-Bu₄NI / 1.) THF, -78 deg C, 5 min, 2.) 10-15 deg C, 45 min

With dmap; ammonia; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00058a005

Reference yield:

: 4326-36-7
(S)-N-(tert-butoxycarbonyl)tyrosine methyl ester

: 147363-14-2
C₃₇H₄₉BrN₂O₁₀

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate, n-Bu₄NI / dimethylformamide / 16 h

2: liquid NH₃ / methanol / 48 h / Ambient temperature

3: 90 percent / i-Pr₂NEt, DMAP, / CH₂Cl₂ / 2 h / Ambient temperature

4: 1.) NaN(TMS)2 / 2.) n-Bu₄NI / 1.) THF, -78 deg C, 5 min, 2.) 10-15 deg C, 45 min

With dmap; ammonia; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00058a005

Reference yield:

: 3417-91-2
L-tyrosine methyl ester HCl

: 147363-14-2
C₃₇H₄₉BrN₂O₁₀

Guidance literature:: Multi-step reaction with 5 steps

1: i-Pr₂NEt / dimethylformamide / 8 h

2: potassium carbonate, n-Bu₄NI / dimethylformamide / 16 h

3: liquid NH₃ / methanol / 48 h / Ambient temperature

4: 90 percent / i-Pr₂NEt, DMAP, / CH₂Cl₂ / 2 h / Ambient temperature

5: 1.) NaN(TMS)2 / 2.) n-Bu₄NI / 1.) THF, -78 deg C, 5 min, 2.) 10-15 deg C, 45 min

With dmap; ammonia; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; potassium carbonate; N-ethyl-N,N-diisopropylamine; tetra-(n-butyl)ammonium iodide; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo00058a005