benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Base Information

Chemical Name:benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside
CAS No.:88559-76-6
Molecular Formula:C₆₁H₆₄O₁₁
Molecular Weight:973.173
Hs Code.:

Synonyms:benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

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Chemical Property of benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

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Technology Process of benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

There total 5 articles about benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 62867-73-6
benzyl 2,3,6-tri-O-benzyl-4-O-(2′,3′-di-O-benzyl-4′,6′-Obenzylidene-β-D-glucopyranosyl)-β-D-glucopyranoside

: 62867-76-9
benzyl 2,3,6-tri-O-benzyl-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

: 88559-76-6
benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With hydrogenchloride; diethyl ether; 3 A molecular sieve; sodium cyanoborohydride; In tetrahydrofuran; dichloromethane; at 0 ℃; for 1h;
DOI:10.1016/0008-6215(83)84014-2

Reference yield:

: 81927-55-1
O-benzyl 2,2,2-trichloroacetimidate

: benzyl 2,3,6-tri-O-benzyl-4-O-(2′,3′-di-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

: 62867-76-9
benzyl 2,3,6-tri-O-benzyl-(2,3,4-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

: 88559-76-6
benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-glucopyranosyl)-β-D-glucopyranoside

Guidance literature:: With trifluorormethanesulfonic acid; In dichloromethane; at 20 ℃; for 1h; Yield given. Yields of byproduct given;
DOI:10.1007/BF00953238

Reference yield:

: 100-39-0
benzyl bromide

: 62867-79-2,88559-76-6,114079-18-4,124814-06-8,145064-87-5
benzyl 2,3,6-tri-O-benzyl-4-O-(2,3,6-tri-O-benzyl-β-D-galactopyranosyl)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent

2: 76 percent / aqueous 80percent acetic acid / 85 °C

3: 60 percent / tetrabutylammonium hydrogensulfate / aq. NaOH / 72 h / Heating

With tetra(n-butyl)ammonium hydrogensulfate; acetic acid; In sodium hydroxide;
DOI:10.1016/0008-6215(87)80191-X