C₂₁H₂₅⁽¹⁸⁾FN₂O₄

Base Information

Chemical Name:C₂₁H₂₅⁽¹⁸⁾FN₂O₄
CAS No.:1383563-23-2
Molecular Formula:C₂₁H₂₅FN₂O₄
Molecular Weight:387.44
Hs Code.:

C<sub>21</sub>H<sub>25</sub><sup>(18)</sup>FN<sub>2</sub>O<sub>4</sub>

Synonyms:C₂₁H₂₅⁽¹⁸⁾FN₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₁H₂₅⁽¹⁸⁾FN₂O₄

Chemical Property:

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Technology Process of C₂₁H₂₅⁽¹⁸⁾FN₂O₄

There total 3 articles about C₂₁H₂₅⁽¹⁸⁾FN₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1383563-20-9
2-(2-(2-((2-(4-(dimethylamino)phenyl)benzo[d]oxazol-5-yl)oxy)-ethoxy)ethoxy)ethyl 4-methylbenzenesulfonate

: 1383563-23-2
C₂₁H₂₅⁽¹⁸⁾FN₂O₄

Guidance literature:: With potassium carbonate; [2.2.2]cryptande; In acetonitrile; at 120 ℃; for 0.1h;
DOI:10.1021/jm300251n

Reference yield:

: 1568-70-3
4-methoxy-2-nitrophenol

: 1383563-23-2
C₂₁H₂₅⁽¹⁸⁾FN₂O₄

Guidance literature:: Multi-step reaction with 6 steps

1: palladium 10% on activated carbon; hydrogen / methanol / 24 h / 20 °C

2: polyphosphoric acid / 0.5 h / 180 °C

3: boron tribromide / dichloromethane / 13 h / -78 - 20 °C / Cooling with acetone-dry ice

4: potassium carbonate / N,N-dimethyl-formamide / 3 h / 110 °C

5: pyridine / 3 h / 20 °C

6: potassium carbonate; [2.2.2]cryptande / acetonitrile / 0.1 h / 120 °C

With palladium 10% on activated carbon; hydrogen; boron tribromide; potassium carbonate; [2.2.2]cryptande; In pyridine; methanol; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm300251n

Reference yield:

: 20734-76-3
2-amino-4-methoxyphenol

: 1383563-23-2
C₂₁H₂₅⁽¹⁸⁾FN₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1: polyphosphoric acid / 0.5 h / 180 °C

2: boron tribromide / dichloromethane / 13 h / -78 - 20 °C / Cooling with acetone-dry ice

3: potassium carbonate / N,N-dimethyl-formamide / 3 h / 110 °C

4: pyridine / 3 h / 20 °C

5: potassium carbonate; [2.2.2]cryptande / acetonitrile / 0.1 h / 120 °C

With boron tribromide; potassium carbonate; [2.2.2]cryptande; In pyridine; dichloromethane; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1021/jm300251n