dicarbonyl(η2-dimethylthiophosphinito)(tricyclohexylphosphane)cobalt(I)

Base Information

Chemical Name:dicarbonyl(η2-dimethylthiophosphinito)(tricyclohexylphosphane)cobalt(I)
CAS No.:112792-43-5
Molecular Formula:C₂₂H₃₉CoO₂P₂S
Molecular Weight:488.557
Hs Code.:

Synonyms:dicarbonyl(η2-dimethylthiophosphinito)(tricyclohexylphosphane)cobalt(I)

Suppliers and Price of dicarbonyl(η2-dimethylthiophosphinito)(tricyclohexylphosphane)cobalt(I)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of dicarbonyl(η2-dimethylthiophosphinito)(tricyclohexylphosphane)cobalt(I)

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of dicarbonyl(η2-dimethylthiophosphinito)(tricyclohexylphosphane)cobalt(I)

There total 3 articles about dicarbonyl(η2-dimethylthiophosphinito)(tricyclohexylphosphane)cobalt(I) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 112792-41-3
ICo(CO)2(P(C₆H₁₁)3)2

: 6591-05-5
dimethylphosphine sulfide

: 7087-68-5
N-ethyl-N,N-diisopropylamine

: N,N-diisopropylethylamine hydroiodide

: oligomeric dicarbonyl(μ-dimethylthiophosphinito-P,S)(tricyclohexylphosphane)cobalt(I)

: 112792-43-5
dicarbonyl(η2-dimethylthiophosphinito)(tricyclohexylphosphane)cobalt(I)

: 2622-14-2
tricyclohexylphosphine

Guidance literature:: In toluene; under N2 or Ar, exclusion of oxygen and moisture, addn. of Me2HPS to a soln. of Co compound in toluene and dropwise addn. of (Et)(i-Pr)2N in toluene at 25°C during 2 h, 8 h; decantation, concd. in vac., addn. of n-hexane, decantation, cooled to -30°C, filtration of pptn., suspension in toluene, filtration (polymeric product), addn. of hexane to the filtrate, crystn. at -30°C; elem. anal.;