11-tert-butoxycarbonylamino-4,8-bis(2-nitrobenzenesulfonyl)-4,8-diazaundecan-1-yl iodide

Base Information

Chemical Name:11-tert-butoxycarbonylamino-4,8-bis(2-nitrobenzenesulfonyl)-4,8-diazaundecan-1-yl iodide
CAS No.:240423-13-6
Molecular Formula:C₂₆H₃₆IN₅O₁₀S₂
Molecular Weight:769.636
Hs Code.:

Synonyms:11-tert-butoxycarbonylamino-4,8-bis(2-nitrobenzenesulfonyl)-4,8-diazaundecan-1-yl iodide

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Chemical Property of 11-tert-butoxycarbonylamino-4,8-bis(2-nitrobenzenesulfonyl)-4,8-diazaundecan-1-yl iodide

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Technology Process of 11-tert-butoxycarbonylamino-4,8-bis(2-nitrobenzenesulfonyl)-4,8-diazaundecan-1-yl iodide

There total 9 articles about 11-tert-butoxycarbonylamino-4,8-bis(2-nitrobenzenesulfonyl)-4,8-diazaundecan-1-yl iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 240423-19-2
methanesulfonic acid 3-[{3-[(3-tert-butoxycarbonylamino-propyl)-(2-nitro-benzenesulfonyl)-amino]-propyl}-(2-nitro-benzenesulfonyl)-amino]-propyl ester

: 240423-13-6
11-tert-butoxycarbonylamino-4,8-bis(2-nitrobenzenesulfonyl)-4,8-diazaundecan-1-yl iodide

Guidance literature:: With sodium iodide; In butanone; at 60 ℃;
DOI:10.1016/S0040-4039(99)00851-5

Reference yield:

: 1694-92-4
2-Nitrobenzenesulfonyl chloride

: 240423-13-6
11-tert-butoxycarbonylamino-4,8-bis(2-nitrobenzenesulfonyl)-4,8-diazaundecan-1-yl iodide

Guidance literature:: Multi-step reaction with 4 steps

1: 99 percent / pyridine / CH₂Cl₂ / 0.17 h / 0 °C

2: 86 percent / Cs₂CO₃; nBu₄NI / acetonitrile / 1.5 h / 60 °C

3: Et₃N / CH₂Cl₂ / 0.17 h / 20 °C

4: NaI / butan-2-one / 1 h / 60 °C

With pyridine; tetra-(n-butyl)ammonium iodide; caesium carbonate; triethylamine; sodium iodide; In dichloromethane; acetonitrile; butanone;
DOI:10.1248/cpb.48.1570

Reference yield:

: 196214-23-0
N-(3-hydroxypropyl)-2-nitrobenzenesulfonamide

: 240423-13-6
11-tert-butoxycarbonylamino-4,8-bis(2-nitrobenzenesulfonyl)-4,8-diazaundecan-1-yl iodide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / Cs₂CO₃; nBu₄NI / acetonitrile / 1.5 h / 60 °C

2: Et₃N / CH₂Cl₂ / 0.17 h / 20 °C

3: NaI / butan-2-one / 1 h / 60 °C

With tetra-(n-butyl)ammonium iodide; caesium carbonate; triethylamine; sodium iodide; In dichloromethane; acetonitrile; butanone;
DOI:10.1248/cpb.48.1570