O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose

Base Information

Chemical Name:O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose
CAS No.:173468-16-1
Molecular Formula:C₅₂H₄₂O₁₅
Molecular Weight:906.896
Hs Code.:

Synonyms:O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose

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Chemical Property of O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose

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Technology Process of O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose

There total 1 articles about O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 552-71-6,78932-92-0,80244-85-5,80244-86-6,83113-52-4,102046-32-2,102046-33-3
D-(+)-xylobiose

: 98-88-4
benzoyl chloride

: 173468-16-1
O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose

: O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-α-D-xylopyranose

Guidance literature:: With pyridine; for 5h; Ambient temperature;
DOI:10.1016/0008-6215(95)00214-E

Reference yield: 86.0%

: 173468-16-1
O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose

: 173468-17-2
O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-2,3-di-O-benzoyl-α-D-xylopyranosyl bromide

Guidance literature:: With hydrogen bromide; acetic acid; In 1,2-dichloro-ethane; for 0.5h; Ambient temperature;
DOI:10.1016/0008-6215(95)00214-E

Reference yield:

: 173468-16-1
O-(2,3,4-tri-O-benzoyl-β-D-xylopyranosyl)-(1<*>4)-1,2,3-tri-O-benzoyl-β-D-xylopyranose

: 6819-07-4
p-nitrophenyl β-D-xylopyranosyl-(1->4)-β-D-xylopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / HBr, AcOH / 1,2-dichloro-ethane / 0.5 h / Ambient temperature

2: 68 percent / K₂CO₃ / acetone / Ambient temperature

3: 92 percent / NaOMe, MeOH / CH₂Cl₂ / 5 h / Ambient temperature

With methanol; hydrogen bromide; sodium methylate; potassium carbonate; acetic acid; In dichloromethane; 1,2-dichloro-ethane; acetone;
DOI:10.1016/0008-6215(95)00214-E