3-{(Z)-2-bromo-3-[N-(5-bromo-2-methylphenyl)-N-tosylamino]prop-1-enyl}benzoic acid

Base Information

Chemical Name:3-{(Z)-2-bromo-3-[N-(5-bromo-2-methylphenyl)-N-tosylamino]prop-1-enyl}benzoic acid
CAS No.:1380159-41-0
Molecular Formula:C₂₄H₂₁Br₂NO₄S
Molecular Weight:579.309
Hs Code.:

Synonyms:3-{(Z)-2-bromo-3-[N-(5-bromo-2-methylphenyl)-N-tosylamino]prop-1-enyl}benzoic acid

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Chemical Property of 3-{(Z)-2-bromo-3-[N-(5-bromo-2-methylphenyl)-N-tosylamino]prop-1-enyl}benzoic acid

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Technology Process of 3-{(Z)-2-bromo-3-[N-(5-bromo-2-methylphenyl)-N-tosylamino]prop-1-enyl}benzoic acid

There total 7 articles about 3-{(Z)-2-bromo-3-[N-(5-bromo-2-methylphenyl)-N-tosylamino]prop-1-enyl}benzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1380159-40-9
N-{(Z)-2-bromo-3-[3-(1,3-dioxolan-2-yl)phenyl]prop-2-enyl}-N-(5-bromo-2-methylphenyl)-4-methylbenzenesulfonamide

: 1380159-41-0
3-{(Z)-2-bromo-3-[N-(5-bromo-2-methylphenyl)-N-tosylamino]prop-1-enyl}benzoic acid

Guidance literature:: With Jones reagent; water; In acetone; at 0 - 20 ℃; for 2h;
DOI:10.1002/chem.201103819

Reference yield:

: N-(5-bromo-2-methylphenyl)-4-methylbenzenesulfonamide

: 1380159-41-0
3-{(Z)-2-bromo-3-[N-(5-bromo-2-methylphenyl)-N-tosylamino]prop-1-enyl}benzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: triphenylphosphine; diethylazodicarboxylate / toluene / 1 h / 0 - 20 °C

2: Jones reagent; water / acetone / 2 h / 0 - 20 °C

With Jones reagent; water; triphenylphosphine; diethylazodicarboxylate; In acetone; toluene;
DOI:10.1002/chem.201103819

Reference yield:

: C₁₁H₉BrO₃

: 1380159-41-0
3-{(Z)-2-bromo-3-[N-(5-bromo-2-methylphenyl)-N-tosylamino]prop-1-enyl}benzoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: diisobutylaluminium hydride / tetrahydrofuran; hexane / 1 h / 0 °C

2: toluene-4-sulfonic acid; orthoformic acid triethyl ester / toluene / 5 h / 40 °C / Molecular sieve

3: triphenylphosphine; diethylazodicarboxylate / toluene / 1 h / 0 - 20 °C

4: Jones reagent; water / acetone / 2 h / 0 - 20 °C

With Jones reagent; water; diisobutylaluminium hydride; toluene-4-sulfonic acid; orthoformic acid triethyl ester; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; hexane; acetone; toluene;
DOI:10.1002/chem.201103819