N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-N-(3-methoxypropyl)-2-nitrobenzenesulfonamide

Base Information

Chemical Name:N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-N-(3-methoxypropyl)-2-nitrobenzenesulfonamide
CAS No.:1392314-27-0
Molecular Formula:C₁₆H₂₅N₃O₇S₂
Molecular Weight:435.522
Hs Code.:

Synonyms:N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-N-(3-methoxypropyl)-2-nitrobenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-N-(3-methoxypropyl)-2-nitrobenzenesulfonamide

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Technology Process of N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-N-(3-methoxypropyl)-2-nitrobenzenesulfonamide

There total 2 articles about N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-N-(3-methoxypropyl)-2-nitrobenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 36865-41-5
3-bromopropanol methyl ether

: 1392314-22-5
N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-2-nitrobenzenesulfonamide

: 1392314-27-0
N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-N-(3-methoxypropyl)-2-nitrobenzenesulfonamide

Guidance literature:: N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-2-nitrobenzenesulfonamide; With caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; for 0.5h;

3-bromopropanol methyl ether; With caesium carbonate; In N,N-dimethyl-formamide; at 20 - 70 ℃; for 73h;

Reference yield:

: 89937-52-0
2-(1,1-Dioxo-thiomorpholin-4-yl)-ethylamine

: 1392314-27-0
N-(2-(1,1-dioxido-4-thiomorpholinyl)ethyl)-N-(3-methoxypropyl)-2-nitrobenzenesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine / dichloromethane / 18 h / 20 °C / Cooling with ice

2.1: caesium carbonate / N,N-dimethyl-formamide / 0.5 h / 20 °C

2.2: 73 h / 20 - 70 °C

With caesium carbonate; triethylamine; In dichloromethane; N,N-dimethyl-formamide;