benzylphosphonic acid benzyl ethyl ester

Base Information

Chemical Name:benzylphosphonic acid benzyl ethyl ester
CAS No.:945933-82-4
Molecular Formula:C₁₆H₁₉O₃P
Molecular Weight:290.299
Hs Code.:

Synonyms:benzylphosphonic acid benzyl ethyl ester

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Chemical Property of benzylphosphonic acid benzyl ethyl ester

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Technology Process of benzylphosphonic acid benzyl ethyl ester

There total 4 articles about benzylphosphonic acid benzyl ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 18933-98-7
benzylphosphonic acid monoethyl ester

: 100-39-0
benzyl bromide

: 945933-82-4
benzylphosphonic acid benzyl ethyl ester

Guidance literature:: With caesium carbonate; In acetonitrile; for 72h; Heating;
DOI:10.1016/j.bmcl.2007.04.026

Reference yield: 80.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 122-52-1
triethyl phosphite

: 945933-82-4
benzylphosphonic acid benzyl ethyl ester

: 78-38-6
ethylphosphonic acid diethyl ester

: 1080-32-6
O,O-diethyl benzylphosphonate

Guidance literature:: benzyl alcohol; triethyl phosphite; at 125 ℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube;

With tetra-(n-butyl)ammonium iodide; In neat (no solvent); at 125 ℃; for 24h; Inert atmosphere; Schlenk technique; Sealed tube;
DOI:10.1039/c8gc00931g

Reference yield: 43.0%

: 100-51-6,185532-71-2
benzyl alcohol

: 122-52-1
triethyl phosphite

: 945933-82-4
benzylphosphonic acid benzyl ethyl ester

: 78-38-6
ethylphosphonic acid diethyl ester

: 2768-31-2
benzyl diethyl phosphite

: 1080-32-6
O,O-diethyl benzylphosphonate

Guidance literature:: With benzyl bromide; In neat (no solvent); at 150 ℃; for 12h; Inert atmosphere; Schlenk technique; Sealed tube; Green chemistry;
DOI:10.1039/c8gc00931g