23-<(allyloxy)methyl>-4,13-dibenzyl-19,28-diethyl-4,13,19,28-tetraza-1,7,10,16,22,25-hexaoxacyclotriacontane

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Chemical Name:23-<(allyloxy)methyl>-4,13-dibenzyl-19,28-diethyl-4,13,19,28-tetraza-1,7,10,16,22,25-hexaoxacyclotriacontane
CAS No.:118974-41-7
Molecular Formula:C₄₂H₇₀N₄O₇
Molecular Weight:743.04
Hs Code.:

Synonyms:23-<(allyloxy)methyl>-4,13-dibenzyl-19,28-diethyl-4,13,19,28-tetraza-1,7,10,16,22,25-hexaoxacyclotriacontane

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Chemical Property of 23-<(allyloxy)methyl>-4,13-dibenzyl-19,28-diethyl-4,13,19,28-tetraza-1,7,10,16,22,25-hexaoxacyclotriacontane

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Technology Process of 23-<(allyloxy)methyl>-4,13-dibenzyl-19,28-diethyl-4,13,19,28-tetraza-1,7,10,16,22,25-hexaoxacyclotriacontane

There total 4 articles about 23-<(allyloxy)methyl>-4,13-dibenzyl-19,28-diethyl-4,13,19,28-tetraza-1,7,10,16,22,25-hexaoxacyclotriacontane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 114719-16-3
4-<(allyloxy)methyl>-1,8-diiodo-3,6-dioxaoctane

: 118974-45-1
{2-[2-(Benzyl-{2-[2-(2-{benzyl-[2-(2-ethylamino-ethoxy)-ethyl]-amino}-ethoxy)-ethoxy]-ethyl}-amino)-ethoxy]-ethyl}-ethyl-amine

: 118974-41-7
23-<(allyloxy)methyl>-4,13-dibenzyl-19,28-diethyl-4,13,19,28-tetraza-1,7,10,16,22,25-hexaoxacyclotriacontane

Guidance literature:: With potassium carbonate; potassium iodide; In acetonitrile; for 24h; Heating;
DOI:10.1021/jo00278a016

Reference yield:

: 118974-46-2
N-[2-(2-hydroxyethoxy)ethyl]acetamide

: 118974-41-7
23-<(allyloxy)methyl>-4,13-dibenzyl-19,28-diethyl-4,13,19,28-tetraza-1,7,10,16,22,25-hexaoxacyclotriacontane

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride

2: anhydrous Na₂CO₃ / toluene / Heating

3: LiAlH₄

4: K₂CO₃, Na₂CO₃, NaI

With lithium aluminium tetrahydride; thionyl chloride; sodium carbonate; potassium carbonate; sodium iodide; In toluene;
DOI:10.1016/0040-4039(88)85282-1

Reference yield:

: 118974-47-3
N-[2-(2-chloroethoxy)ethyl]acetamide. N-[2-(2-hydroxyethoxy)ethyl]acetamide

: 118974-41-7
23-<(allyloxy)methyl>-4,13-dibenzyl-19,28-diethyl-4,13,19,28-tetraza-1,7,10,16,22,25-hexaoxacyclotriacontane

Guidance literature:: Multi-step reaction with 3 steps

1: anhydrous Na₂CO₃ / toluene / Heating

2: LiAlH₄

3: K₂CO₃, Na₂CO₃, NaI

With lithium aluminium tetrahydride; sodium carbonate; potassium carbonate; sodium iodide; In toluene;
DOI:10.1016/0040-4039(88)85282-1