tri(p-tolyl)bismuth dichloride

Base Information

Chemical Name:tri(p-tolyl)bismuth dichloride
CAS No.:6729-64-2
Molecular Formula:C₂₁H₂₁BiCl₂
Molecular Weight:553.284
Hs Code.:

Synonyms:tri(p-tolyl)bismuth dichloride

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Chemical Property of tri(p-tolyl)bismuth dichloride

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Technology Process of tri(p-tolyl)bismuth dichloride

There total 7 articles about tri(p-tolyl)bismuth dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: (p-Tol)3Bi=C(CO₂Me){C(CO₂Me)=NSO₂Ph}

: 6729-64-2
tri(p-tolyl)bismuth dichloride

Guidance literature:: With H₂O; In dichloromethane; byproducts: CH3OC(O)CHC(C(O)OCH3)NHSO2C6H5; aq. HCl added to CH2Cl2 soln. of Bi compd. (molar ratio 2.9:1); stirredfor 30 min at room temp.; org. phase sepd.; dried over MgSO4; evapd.; Z isomer of dimethyl 2-(N-(phenylsulfonyl))aminofumarate isolated by column chromy. (silica gel); detd. by (1)H NMR;
DOI:10.1016/S0022-328X(00)00295-3

Reference yield: 81.0%

: 7647-01-0,15364-23-5
hydrogenchloride

: 858520-08-8
μ-oxobis[(2,4-dimethylbenzenesulfonato)tri-p-tolylbismuth]

: 6729-64-2
tri(p-tolyl)bismuth dichloride

: 5142-75-6
tri(p-tolyl)bismuth

Guidance literature:: With KOH; In ethanol; byproducts: potassium 2,4-dimethylbenzenesulfonate; Bi compd. treated with a soln. of KOH in EtOH, reacted for 24 h, solvent-removed, extd. (EtOH), treated with HCl in EtOH;
DOI:10.1007/s11176-005-0011-x