1-(2-benzyloxy-3,4-dimethoxyphenethyl)-5-(1,1-ethylenedithioethyl)-2(1H)-pyridinone

Base Information

Chemical Name:1-(2-benzyloxy-3,4-dimethoxyphenethyl)-5-(1,1-ethylenedithioethyl)-2(1H)-pyridinone
CAS No.:89680-86-4
Molecular Formula:C₂₆H₂₉NO₄S₂
Molecular Weight:483.653
Hs Code.:

Synonyms:1-(2-benzyloxy-3,4-dimethoxyphenethyl)-5-(1,1-ethylenedithioethyl)-2(1H)-pyridinone

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Chemical Property of 1-(2-benzyloxy-3,4-dimethoxyphenethyl)-5-(1,1-ethylenedithioethyl)-2(1H)-pyridinone

Chemical Property:

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Technology Process of 1-(2-benzyloxy-3,4-dimethoxyphenethyl)-5-(1,1-ethylenedithioethyl)-2(1H)-pyridinone

There total 7 articles about 1-(2-benzyloxy-3,4-dimethoxyphenethyl)-5-(1,1-ethylenedithioethyl)-2(1H)-pyridinone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 56774-68-6
2'-benzyloxy-3',4'-dimethoxyacetophenone

: 89680-86-4
1-(2-benzyloxy-3,4-dimethoxyphenethyl)-5-(1,1-ethylenedithioethyl)-2(1H)-pyridinone

Guidance literature:: Multi-step reaction with 7 steps

1: 62 percent / sulfur / 80 degC, 1 h then reflux, 4 h

2: 93 percent / 50percent KOH, HCl / H₂O; ethanol / 9 h / Heating

3: 97 percent / 10percent HCl / 20 h / Ambient temperature

4: 97 percent / LiAlH₄ / diethyl ether / 4 h / Ambient temperature

5: 88 percent / triphenylphosphine, N-bromosuccinimide / benzene / 2 h / Ambient temperature

6: 94 percent / benzene / 72 h / Heating

7: potassium ferricyanide, KOH

With hydrogenchloride; potassium hydroxide; N-Bromosuccinimide; lithium aluminium tetrahydride; sulfur; triphenylphosphine; potassium hexacyanoferrate(III); In diethyl ether; ethanol; water; benzene;
DOI:10.1248/cpb.33.5316

Reference yield:

: 79659-43-1
2'-benzyloxy-3',4'-dimethoxyphenylacetic acid

: 89680-86-4
1-(2-benzyloxy-3,4-dimethoxyphenethyl)-5-(1,1-ethylenedithioethyl)-2(1H)-pyridinone

Guidance literature:: Multi-step reaction with 5 steps

1: 97 percent / 10percent HCl / 20 h / Ambient temperature

2: 97 percent / LiAlH₄ / diethyl ether / 4 h / Ambient temperature

3: 88 percent / triphenylphosphine, N-bromosuccinimide / benzene / 2 h / Ambient temperature

4: 94 percent / benzene / 72 h / Heating

5: potassium ferricyanide, KOH

With hydrogenchloride; potassium hydroxide; N-Bromosuccinimide; lithium aluminium tetrahydride; triphenylphosphine; potassium hexacyanoferrate(III); In diethyl ether; benzene;
DOI:10.1248/cpb.33.5316

Reference yield:

: 89680-84-2
2-benzyloxy-3,4-dimethoxyphenethyl-bromide

: 89680-86-4
1-(2-benzyloxy-3,4-dimethoxyphenethyl)-5-(1,1-ethylenedithioethyl)-2(1H)-pyridinone

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / benzene / 72 h / Heating

2: potassium ferricyanide, KOH

With potassium hydroxide; potassium hexacyanoferrate(III); In benzene;
DOI:10.1248/cpb.33.5316