C₁₉H₂₂OSi

Base Information

• Chemical Name: C₁₉H₂₂OSi
• CAS No.: 1292811-35-8
• Molecular Formula: C₁₉H₂₂OSi
• Molecular Weight: 294.469
• Mol file: 1292811-35-8.mol

Synonyms:C₁₉H₂₂OSi

Chemical Property of C₁₉H₂₂OSi

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₁₉H₂₂OSi

There total 1 articles about C₁₉H₂₂OSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

diphenylsilyl chloride (1631-83-0) + 2-methyl-4-hexyl-2-ol (857765-94-7) → C19H22OSi (1292811-35-8)

Guidance literature:

With triethylamine; In dichloromethane; at 0 - 20 ℃; for 2h; Inert atmosphere;

DOI:10.1021/ja200712f

Reference yield: 99.0%

carbon monoxide (201230-82-2) + C19H22OSi (1292811-35-8) → C20H22O2Si

Guidance literature:

dicarbonylacetylacetonato rhodium (I); In dichloromethane; for 15h; under 31029.7 Torr;

Reference yield:

C19H22OSi (1292811-35-8) → C24H30O2Si

Guidance literature:

Multi-step reaction with 2 steps

1.1: dicarbonylacetylacetonato rhodium (I) / dichloromethane / 15 h / 20 °C / 31029.7 Torr / Inert atmosphere

2.1: scandium tris(trifluoromethanesulfonate) / dichloromethane / 3 h / 20 °C / Inert atmosphere

2.2: 0.5 h / 20 °C / Inert atmosphere

With dicarbonylacetylacetonato rhodium (I); scandium tris(trifluoromethanesulfonate); In dichloromethane;

DOI:10.1021/ja200712f

upstream raw materials:

diphenylsilyl chloride

2-methyl-4-hexyl-2-ol