9,10-dioxa-syn-(2-((N-(3-methylphenyl)amino)sulfonyl)ethyl,methyl)(ethyl,methyl)bimane

Base Information

Chemical Name:9,10-dioxa-syn-(2-((N-(3-methylphenyl)amino)sulfonyl)ethyl,methyl)(ethyl,methyl)bimane
CAS No.:129065-69-6
Molecular Formula:C₁₉H₂₃N₃O₄S
Molecular Weight:389.475
Hs Code.:

Synonyms:9,10-dioxa-syn-(2-((N-(3-methylphenyl)amino)sulfonyl)ethyl,methyl)(ethyl,methyl)bimane

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Chemical Property of 9,10-dioxa-syn-(2-((N-(3-methylphenyl)amino)sulfonyl)ethyl,methyl)(ethyl,methyl)bimane

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Technology Process of 9,10-dioxa-syn-(2-((N-(3-methylphenyl)amino)sulfonyl)ethyl,methyl)(ethyl,methyl)bimane

There total 8 articles about 9,10-dioxa-syn-(2-((N-(3-methylphenyl)amino)sulfonyl)ethyl,methyl)(ethyl,methyl)bimane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 129065-41-4
9,10-dioxa-syn-(2-(chlorosulfonyl)ethyl,methyl)(ethyl,methyl)bimane

: 108-44-1
1-amino-3-methylbenzene

: 129065-69-6
9,10-dioxa-syn-(2-((N-(3-methylphenyl)amino)sulfonyl)ethyl,methyl)(ethyl,methyl)bimane

Guidance literature:: In acetonitrile; for 12h; Ambient temperature; other temp. and time;
DOI:10.1021/ja00176a034

Reference yield:

: 88848-54-8
3-(1-Bromo-ethyl)-5-ethyl-2,6-dimethyl-pyrazolo[1,2-a]pyrazole-1,7-dione

: 129065-69-6
9,10-dioxa-syn-(2-((N-(3-methylphenyl)amino)sulfonyl)ethyl,methyl)(ethyl,methyl)bimane

Guidance literature:: Multi-step reaction with 6 steps

1: 90.3 percent / tetrahydrofuran / 0.33 h / Ambient temperature

2: 100 percent / 3-chloroperbenzoic acid / CH₂Cl₂ / 0.25 h / 0 °C

3: 84 percent / benzene / 4 h / Heating

4: 95 percent / sodium bisulfite / acetonitrile; H₂O / 2 h / Heating

5: 94 percent / SOCl₂, DMF / CH₂Cl₂ / 0.5 h / Ambient temperature

6: 75 percent / acetonitrile / 12 h / Ambient temperature; other temp. and time

With thionyl chloride; sodium hydrogensulfite; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; dichloromethane; water; acetonitrile; benzene;
DOI:10.1021/ja00176a034

Reference yield:

: 129065-34-5
9,10-dioxa-syn-(vinyl,methyl)(ethyl,methyl)bimane

: 129065-69-6
9,10-dioxa-syn-(2-((N-(3-methylphenyl)amino)sulfonyl)ethyl,methyl)(ethyl,methyl)bimane

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / sodium bisulfite / acetonitrile; H₂O / 2 h / Heating

2: 94 percent / SOCl₂, DMF / CH₂Cl₂ / 0.5 h / Ambient temperature

3: 75 percent / acetonitrile / 12 h / Ambient temperature; other temp. and time

With thionyl chloride; sodium hydrogensulfite; N,N-dimethyl-formamide; In dichloromethane; water; acetonitrile;
DOI:10.1021/ja00176a034