Technology Process of C19H14O2
There total 5 articles about C19H14O2 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
o-tetrachloroquinone;
In
chloroform;
at 0 - 20 ℃;
Inert atmosphere;
DOI:10.1021/ol200808q
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: n-butyllithium / tetrahydrofuran; hexane / 0.33 h / -78 °C / Inert atmosphere
1.2: -78 - 20 °C / Inert atmosphere
2.1: sodium tetrahydroborate; trifluoroacetic acid / 0.17 h / 0 °C
3.1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere
4.1: o-tetrachloroquinone / chloroform / 0 - 20 °C / Inert atmosphere
With
sodium tetrahydroborate; n-butyllithium; o-tetrachloroquinone; boron tribromide; trifluoroacetic acid;
In
tetrahydrofuran; hexane; dichloromethane; chloroform;
DOI:10.1021/ol200808q
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron tribromide / dichloromethane / -78 - 20 °C / Inert atmosphere
2: o-tetrachloroquinone / chloroform / 0 - 20 °C / Inert atmosphere
With
o-tetrachloroquinone; boron tribromide;
In
dichloromethane; chloroform;
DOI:10.1021/ol200808q