2-Hydroxybenzoic acid 2-[(4-nitrophenyl)methylene]hydrazide

Base Information

Chemical Name:2-Hydroxybenzoic acid 2-[(4-nitrophenyl)methylene]hydrazide
CAS No.:72323-41-2
Molecular Formula:C₁₄H₁₁N₃O₄
Molecular Weight:285.259
Hs Code.:
DSSTox Substance ID:DTXSID501189844

Synonyms:CBDivE_002046;DTXSID501189844;2-Hydroxybenzoic acid 2-[(4-nitrophenyl)methylene]hydrazide;72323-41-2

Suppliers and Price of 2-Hydroxybenzoic acid 2-[(4-nitrophenyl)methylene]hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2-Hydroxybenzoic acid 2-[(4-nitrophenyl)methylene]hydrazide

Chemical Property:

XLogP3:2.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:5
Rotatable Bond Count:3
Exact Mass:285.07495584
Heavy Atom Count:21
Complexity:400

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)NN=CC2=CC=C(C=C2)[N+](=O)[O-])O

Technology Process of 2-Hydroxybenzoic acid 2-[(4-nitrophenyl)methylene]hydrazide

There total 8 articles about 2-Hydroxybenzoic acid 2-[(4-nitrophenyl)methylene]hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 555-16-8
4-nitrobenzaldehdye

: 936-02-7
2-Hydroxybenzoylhydrazine

: 72323-41-2
N'-[(4-nitrophenyl)methylidene]-2-hydroxybenzohydrazide

Guidance literature:: In ethanol; for 5h; Reflux;
DOI:10.1016/j.tetlet.2014.12.037

Reference yield:

: 118-61-6
2-hydroxy-benzoic acid ethyl ester

: 72323-41-2
N'-[(4-nitrophenyl)methylidene]-2-hydroxybenzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / Reflux

2: ethanol / Reflux

With hydrazine hydrate; In ethanol;
DOI:10.1016/j.molstruc.2021.132058

Reference yield:

: 70203-02-0
N'-(2-phenyl-2-ethylidene)-2-hydroxybenzohydrazide

: 72323-41-2
N'-[(4-nitrophenyl)methylidene]-2-hydroxybenzohydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid / water

2: acetic acid / ethanol / Reflux

With sulfuric acid; acetic acid; In ethanol; water;
DOI:10.1002/jhet.2516