Technology Process of C26H27FN4O6S
There total 2 articles about C26H27FN4O6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
acetic acid; sodium sulfate;
In
tetrahydrofuran; acetonitrile;
at 35 ℃;
for 3h;
- Guidance literature:
-
C26H29FN4O6S;
With
sodium hypochlorite; acetic acid;
In
ethyl acetate; tert-butyl alcohol;
at 5 - 10 ℃;
Industry scale;
With
1,8-diazabicyclo[5.4.0]undec-7-ene;
In
ethyl acetate; tert-butyl alcohol;
at 5 - 10 ℃;
for 0.666667h;
Industry scale;
- Guidance literature:
-
C26H27FN4O6S;
With
titanium(IV) isopropylate; dichloro-acetic acid; hydrogen;
bis(norbornadiene)rhodium(l)tetrafluoroborate;
In
dichloromethane; 2,2,2-trifluoroethanol;
at 25 ℃;
for 18h;
under 5931.67 Torr;
Industry scale;
Autoclave;
Inert atmosphere;
With
potassium hydrogene glycolate;
In
dichloromethane; 2,2,2-trifluoroethanol; isopropyl alcohol;
at 20 - 25 ℃;
for 2h;
Industry scale;
Inert atmosphere;
toluene-4-sulfonic acid;
In
dichloromethane; 2,2,2-trifluoroethanol; isopropyl alcohol;
at 20 - 60 ℃;
Inert atmosphere;
Industry scale;