methyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate

Base Information

Chemical Name:methyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate
CAS No.:1401065-87-9
Molecular Formula:C₁₈H₁₈BrN₃O₂
Molecular Weight:388.264
Hs Code.:

Synonyms:methyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate

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Chemical Property of methyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate

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Technology Process of methyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate

There total 5 articles about methyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1401065-82-4
tert-butyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate

: 1401065-87-9
methyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 2h;
DOI:10.1039/c2cc34533a

Reference yield:

: 68790-38-5
2-(tert-butyloxycarbonylamino)benzoic acid

: 1401065-87-9
methyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 2 steps

1: ethylene dichloride hydrochloride; benzotriazol-1-ol / dichloromethane / 12 h / 20 °C

2: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C

With ethylene dichloride hydrochloride; benzotriazol-1-ol; trifluoroacetic acid; In dichloromethane;
DOI:10.1039/c3ob41967c

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 1401065-87-9
methyl (S)-2-(2-(4-bromophenylcarbamoyl)pyrrolidine-1-carbonyl)phenylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / 1,4-dioxane; water / 3 h / 20 °C

2: ethylene dichloride hydrochloride; benzotriazol-1-ol / dichloromethane / 12 h / 20 °C

3: trifluoroacetic acid / dichloromethane / 3 h / 0 - 20 °C

With ethylene dichloride hydrochloride; benzotriazol-1-ol; trifluoroacetic acid; sodium hydroxide; In 1,4-dioxane; dichloromethane; water;
DOI:10.1039/c3ob41967c