(E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Base Information

Chemical Name:(E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide
CAS No.:1445726-78-2
Molecular Formula:C₁₈H₁₉N₃O₁₀S
Molecular Weight:469.429
Hs Code.:

Synonyms:(E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Suppliers and Price of (E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

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Technology Process of (E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

There total 6 articles about (E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 49.0%

: 830-79-5
2,4,6-trimethoxybenzaldehyde

: 1445727-02-5
2-(N-(4-methoxy-3,5-dinitrophenyl)sulfamoyl)acetic acid

: 1445726-78-2
(E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Guidance literature:: With acetic acid; benzylamine; at 20 ℃; for 8h; Reflux; Inert atmosphere;
DOI:10.1021/jm400575x

Reference yield:

: 456-22-4
4-Fluorobenzoic acid

: 1445726-78-2
(E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Guidance literature:: Multi-step reaction with 6 steps

1: sulfuric acid; nitric acid / 3 h / 95 °C / Inert atmosphere

2: sulfuric acid; sodium azide / 1,2-dichloro-ethane / 1 h / Reflux; Inert atmosphere

3: potassium hydroxide / 0.5 h / 20 °C / Inert atmosphere

4: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

5: sodium hydroxide / water / 3 h / 20 °C / Inert atmosphere

6: acetic acid; benzylamine / 8 h / 20 °C / Reflux; Inert atmosphere

With sodium azide; sulfuric acid; nitric acid; acetic acid; triethylamine; benzylamine; potassium hydroxide; sodium hydroxide; In dichloromethane; water; 1,2-dichloro-ethane;
DOI:10.1021/jm400575x

Reference yield:

: 92367-07-2
3,5-dinitro-4-fluoro aniline

: 1445726-78-2
(E)-N-(4-methoxy-3,5-dinitrophenyl)-2-(2,4,6-trimethoxyphenyl)ethenesulfonamide

Guidance literature:: Multi-step reaction with 4 steps

1: potassium hydroxide / 0.5 h / 20 °C / Inert atmosphere

2: triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

3: sodium hydroxide / water / 3 h / 20 °C / Inert atmosphere

4: acetic acid; benzylamine / 8 h / 20 °C / Reflux; Inert atmosphere

With acetic acid; triethylamine; benzylamine; potassium hydroxide; sodium hydroxide; In dichloromethane; water;
DOI:10.1021/jm400575x