4-[1-(tetrahydrofuran-2-ylmethyl)-1H-[1,2,3]triazol-4-ylmethoxy]benzaldehyde

Base Information

Chemical Name:4-[1-(tetrahydrofuran-2-ylmethyl)-1H-[1,2,3]triazol-4-ylmethoxy]benzaldehyde
CAS No.:1322786-90-2
Molecular Formula:C₁₅H₁₇N₃O₃
Molecular Weight:287.318
Hs Code.:

Synonyms:4-[1-(tetrahydrofuran-2-ylmethyl)-1H-[1,2,3]triazol-4-ylmethoxy]benzaldehyde

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Chemical Property of 4-[1-(tetrahydrofuran-2-ylmethyl)-1H-[1,2,3]triazol-4-ylmethoxy]benzaldehyde

Chemical Property:

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Technology Process of 4-[1-(tetrahydrofuran-2-ylmethyl)-1H-[1,2,3]triazol-4-ylmethoxy]benzaldehyde

There total 2 articles about 4-[1-(tetrahydrofuran-2-ylmethyl)-1H-[1,2,3]triazol-4-ylmethoxy]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 5651-86-5
4-(prop-2-ynyloxy)benzaldehyde

: 34583-63-6
rac-(tetrahydrofuran-2-yl)methyl 4-methylbenzenesulfonate

: 1322786-90-2
4-[1-(tetrahydrofuran-2-ylmethyl)-1H-[1,2,3]triazol-4-ylmethoxy]benzaldehyde

Guidance literature:: rac-(tetrahydrofuran-2-yl)methyl 4-methylbenzenesulfonate; With sodium azide; In water; N,N-dimethyl-formamide; at 80 ℃; for 4h;

4-(prop-2-ynyloxy)benzaldehyde; With (3-hydroxy-3-phenyl-2-propenedithioate S,S′)bis(triphenylphosphine-P)copper(I); In methanol; water; N,N-dimethyl-formamide;
DOI:10.1080/00397911.2010.516052

Reference yield:

: 97-99-4
Tetrahydrofurfuryl alcohol

: 1322786-90-2
4-[1-(tetrahydrofuran-2-ylmethyl)-1H-[1,2,3]triazol-4-ylmethoxy]benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 1,2-dichloro-ethane / 4 h / 30 - 60 °C

2: sodium azide / water; N,N-dimethyl-formamide / 4 h / 80 °C

With pyridine; sodium azide; In water; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1080/00397911.2010.516052