C₁₅H₁₅ClFN₃O

Base Information

Chemical Name:C₁₅H₁₅ClFN₃O
CAS No.:1383735-73-6
Molecular Formula:C₁₅H₁₅ClFN₃O
Molecular Weight:307.755
Hs Code.:

C<sub>15</sub>H<sub>15</sub>ClFN<sub>3</sub>O

Synonyms:C₁₅H₁₅ClFN₃O

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Chemical Property of C₁₅H₁₅ClFN₃O

Chemical Property:

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Technology Process of C₁₅H₁₅ClFN₃O

There total 7 articles about C₁₅H₁₅ClFN₃O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 75-44-5
phosgene

: 1383735-62-3
1-(4-fluorophenyl)-5,5-dimethyl-4,5,6,7-tetrahydro-1-pyrazolo[4,3-b]pyridine

: 1383735-73-6
C₁₅H₁₅ClFN₃O

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; water; toluene; for 2.5h;

Reference yield:

: 1383735-78-1
C₁₂H₉FN₂O

: 1383735-73-6
C₁₅H₁₅ClFN₃O

Guidance literature:: Multi-step reaction with 7 steps

1: tetrahydrofuran / 18 h

2: perchloric acid; N-bromoacetamide / tetrahydrofuran / 18 h / 0 °C

3: titanium(IV) isopropylate / tetrahydrofuran / 18 h / 60 °C

4: tetrahydrofuran / 2 h / -78 - 20 °C

5: hydrogenchloride / 1,4-dioxane; methanol / 2 h

6: sodium t-butanolate / bis(dibenzylideneacetone)-palladium⁽⁰⁾; tert-butyl XPhos / toluene / 8 h / 100 °C / Inert atmosphere

7: sodium hydrogencarbonate / dichloromethane; toluene; water / 2.5 h

With titanium(IV) isopropylate; hydrogenchloride; perchloric acid; sodium hydrogencarbonate; sodium t-butanolate; N-bromoacetamide; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tert-butyl XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene;

Reference yield:

: 1383735-17-8
C₁₇H₂₁BrFN₃OS

: 1383735-73-6
C₁₅H₁₅ClFN₃O

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 2 h / -78 - 20 °C

2: hydrogenchloride / 1,4-dioxane; methanol / 2 h

3: sodium t-butanolate / bis(dibenzylideneacetone)-palladium⁽⁰⁾; tert-butyl XPhos / toluene / 8 h / 100 °C / Inert atmosphere

4: sodium hydrogencarbonate / dichloromethane; toluene; water / 2.5 h

With hydrogenchloride; sodium hydrogencarbonate; sodium t-butanolate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; tert-butyl XPhos; In tetrahydrofuran; 1,4-dioxane; methanol; dichloromethane; water; toluene;