Technology Process of (S)-3-[4-((S)-2,3-Dihydroxy-propoxy)-phenoxy]-propane-1,2-diol
There total 3 articles about (S)-3-[4-((S)-2,3-Dihydroxy-propoxy)-phenoxy]-propane-1,2-diol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III);
In
water; tert-butyl alcohol;
at 0 ℃;
for 15h;
DOI:10.1021/jo971324h
- Guidance literature:
-
With
potassium osmate(VI); (DHQD)2AQN; potassium carbonate; potassium hexacyanoferrate(III);
In
water; tert-butyl alcohol;
Product distribution;
other reactants: 1,4-bis(5-hexenyl-, and 7-octenyloxy)benzenes, 5-hexen-1-ol, other reagents: K3Fe(CN)6 or I2/(DHQD)2-PHAL or (DHQD)2-PYR or (DHQD)2-AQN/K2CO3/K2OsO4*2H2O;
DOI:10.1021/jo980844p
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 95 percent / K2CO3 / acetone / 5 h / Heating
2: 80 percent / (DHQD)2-PHAL, potassium ferricyanide, K2CO3 / 2-methyl-propan-2-ol; H2O / 15 h / 0 °C
With
potassium carbonate; 1,4-bis(9-O-dihydroquinidine)phthalazine; potassium hexacyanoferrate(III);
In
water; acetone; tert-butyl alcohol;
DOI:10.1021/jo971324h
