phosphoric acid (2R,3S)-2,3-bis-benzyloxy-4-oxo-butyl ester diphenyl ester

Base Information

Chemical Name:phosphoric acid (2R,3S)-2,3-bis-benzyloxy-4-oxo-butyl ester diphenyl ester
CAS No.:872130-25-1
Molecular Formula:C₃₀H₂₉O₇P
Molecular Weight:532.53
Hs Code.:

Synonyms:phosphoric acid (2R,3S)-2,3-bis-benzyloxy-4-oxo-butyl ester diphenyl ester

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Chemical Property of phosphoric acid (2R,3S)-2,3-bis-benzyloxy-4-oxo-butyl ester diphenyl ester

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Technology Process of phosphoric acid (2R,3S)-2,3-bis-benzyloxy-4-oxo-butyl ester diphenyl ester

There total 4 articles about phosphoric acid (2R,3S)-2,3-bis-benzyloxy-4-oxo-butyl ester diphenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 872130-24-0
phosphoric acid (2R,3R)-2,3-bis-benzyloxy-4-hydroxy-butyl ester diphenyl ester

: 872130-25-1
phosphoric acid (2R,3S)-2,3-bis-benzyloxy-4-oxo-butyl ester diphenyl ester

Guidance literature:: With Dess-Martin periodane; In dichloromethane; for 4h; Heating;
DOI:10.1039/b511661a

Reference yield:

: 100-39-0
benzyl bromide

: 872130-25-1
phosphoric acid (2R,3S)-2,3-bis-benzyloxy-4-oxo-butyl ester diphenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 97 percent / Ag₂O; KI / CH₂Cl₂ / 1 h / Heating

2: 76 percent / LiAlH₄ / diethyl ether / 4 h / Heating

3: 48 percent / imidazole / CH₂Cl₂ / 4 h / 0 °C

4: 87 percent / Dess-Martin periodinane / CH₂Cl₂ / 4 h / Heating

With 1H-imidazole; lithium aluminium tetrahydride; Dess-Martin periodane; potassium iodide; silver(l) oxide; In diethyl ether; dichloromethane;
DOI:10.1039/b511661a

Reference yield:

: 113350-84-8
(2R,3R)-(-)-2,3-bis(phenylmethoxy)-1,4-butanediol

: 872130-25-1
phosphoric acid (2R,3S)-2,3-bis-benzyloxy-4-oxo-butyl ester diphenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / imidazole / CH₂Cl₂ / 4 h / 0 °C

2: 87 percent / Dess-Martin periodinane / CH₂Cl₂ / 4 h / Heating

With 1H-imidazole; Dess-Martin periodane; In dichloromethane;
DOI:10.1039/b511661a