6,7-dimethoxy-2-(3-(3,4,5-trimethoxyphenyl)-2-propenylidene)-1-tetralone

Base Information

Chemical Name:6,7-dimethoxy-2-(3-(3,4,5-trimethoxyphenyl)-2-propenylidene)-1-tetralone
CAS No.:1594880-55-3
Molecular Formula:C₂₄H₂₆O₆
Molecular Weight:410.467
Hs Code.:

Synonyms:6,7-dimethoxy-2-(3-(3,4,5-trimethoxyphenyl)-2-propenylidene)-1-tetralone

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Chemical Property of 6,7-dimethoxy-2-(3-(3,4,5-trimethoxyphenyl)-2-propenylidene)-1-tetralone

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Technology Process of 6,7-dimethoxy-2-(3-(3,4,5-trimethoxyphenyl)-2-propenylidene)-1-tetralone

There total 2 articles about 6,7-dimethoxy-2-(3-(3,4,5-trimethoxyphenyl)-2-propenylidene)-1-tetralone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 27.0%

: 34346-90-2
3-(3',4',5'-trimethoxyphenyl)-prop-2-en-1-al

: 13575-75-2
6,7-dimethoxy-1-oxo-1,2,3,4-tetrahydronaphthalene

: 1594880-55-3
6,7-dimethoxy-2-(3-(3,4,5-trimethoxyphenyl)-2-propenylidene)-1-tetralone

Guidance literature:: 6,7-dimethoxy-1-oxo-1,2,3,4-tetrahydronaphthalene; With sodium hydroxide; In ethanol; at 20 ℃; for 0.5h;

3-(3',4',5'-trimethoxyphenyl)-prop-2-en-1-al; In ethanol; at 20 ℃;
DOI:10.1016/j.bmc.2014.02.005

Reference yield:

: 86-81-7
3,4,5-trimethoxy-benzaldehyde

: 1594880-55-3
6,7-dimethoxy-2-(3-(3,4,5-trimethoxyphenyl)-2-propenylidene)-1-tetralone

Guidance literature:: Multi-step reaction with 2 steps

1.1: 18-crown-6 ether; sodium hydride / tetrahydrofuran / 20 °C / Inert atmosphere

2.1: sodium hydroxide / ethanol / 0.5 h / 20 °C

2.2: 20 °C

With 18-crown-6 ether; sodium hydride; sodium hydroxide; In tetrahydrofuran; ethanol; 2.1: |Claisen-Schmidt Condensation / 2.2: |Claisen-Schmidt Condensation;
DOI:10.1016/j.bmc.2014.02.005