Technology Process of 7-O-(heptaacetyl-β-D-cellobiosyl)apigenin
There total 5 articles about 7-O-(heptaacetyl-β-D-cellobiosyl)apigenin which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: silver (II) carbonate; quinoline / 3 h / 20 °C
2: sulfuric acid / 3 h / 20 °C / Cooling with ice
3: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 2.25 h
4: methanol; ammonium acetate / water; tetrahydrofuran / 24 h / 50 °C
With
quinoline; methanol; silver (II) carbonate; N-Bromosuccinimide; sulfuric acid; ammonium acetate; dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane; water;
1: |Koenigs-Knorr Glycosidation;
DOI:10.1080/14786419.2012.686908
- Guidance literature:
-
Multi-step reaction with 3 steps
1: sulfuric acid / 3 h / 20 °C / Cooling with ice
2: N-Bromosuccinimide; dibenzoyl peroxide / tetrachloromethane / 2.25 h
3: methanol; ammonium acetate / water; tetrahydrofuran / 24 h / 50 °C
With
methanol; N-Bromosuccinimide; sulfuric acid; ammonium acetate; dibenzoyl peroxide;
In
tetrahydrofuran; tetrachloromethane; water;
DOI:10.1080/14786419.2012.686908
