bis(trimethylsilyl) 3-indolyl(p-ethoxycarbonylphenylamino)methylphosphonate

Base Information

Chemical Name:bis(trimethylsilyl) 3-indolyl(p-ethoxycarbonylphenylamino)methylphosphonate
CAS No.:479622-59-8
Molecular Formula:C₂₄H₃₅N₂O₅PSi₂
Molecular Weight:518.697
Hs Code.:

Synonyms:bis(trimethylsilyl) 3-indolyl(p-ethoxycarbonylphenylamino)methylphosphonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of bis(trimethylsilyl) 3-indolyl(p-ethoxycarbonylphenylamino)methylphosphonate

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Technology Process of bis(trimethylsilyl) 3-indolyl(p-ethoxycarbonylphenylamino)methylphosphonate

There total 3 articles about bis(trimethylsilyl) 3-indolyl(p-ethoxycarbonylphenylamino)methylphosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 91775-26-7
bis(trimethylsilyl) hydrogen phosphite

: 329721-62-2
ethyl N-(3-indolylmethylene)-p-aminobenzoate

: 479622-59-8
bis(trimethylsilyl) 3-indolyl(p-ethoxycarbonylphenylamino)methylphosphonate

Guidance literature:: In benzene; at 70 - 80 ℃; for 5h;
DOI:10.1023/A:1019671324617

Reference yield:

: 487-89-8,1228547-52-1
Indole-3-carboxaldehyde

: 479622-59-8
bis(trimethylsilyl) 3-indolyl(p-ethoxycarbonylphenylamino)methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / 2 h / 90 - 100 °C

2: 59 percent / benzene / 5 h / 70 - 80 °C

In benzene;
DOI:10.1023/A:1019671324617

Reference yield:

: 94-09-7
p-aminoethylbenzoate

: 479622-59-8
bis(trimethylsilyl) 3-indolyl(p-ethoxycarbonylphenylamino)methylphosphonate

Guidance literature:: Multi-step reaction with 2 steps

1: 65 percent / 2 h / 90 - 100 °C

2: 59 percent / benzene / 5 h / 70 - 80 °C

In benzene;
DOI:10.1023/A:1019671324617