[Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]ClO₄

Base Information

• Chemical Name: [Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]ClO₄
• CAS No.: 112312-54-6
• Molecular Formula: C₃₅H₃₄NOPRh*ClO₄
• Molecular Weight: 717.991
• Mol file: 112312-54-6.mol

Synonyms:[Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]ClO₄

Chemical Property of [Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]ClO₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]ClO₄

There total 4 articles about [Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]⁽¹⁺⁾*ClO₄^(1-)=[Rh(C₈H₁₂)(C₉H₇NO)(P(C₆H₅)3)]ClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

[Rh(C8H12)(C9H7NO)2](1+)*ClO4(1-)=[Rh(C8H12)(C9H7NO)2]ClO4 (112312-48-8) → [Rh(C8H12)(C9H7NO)(P(C6H5)3)](1+)*ClO4(1-)=[Rh(C8H12)(C9H7NO)(P(C6H5)3)]ClO4 (112312-54-6)

Guidance literature:

With triphenylphosphine; In not given; 25°C, stoichiometric amts.; elem. anal.;

DOI:10.1016/S0020-1693(00)81246-3

Reference yield:

isoquinoline-N-oxide hydrate (54243-41-3) → [Rh(C8H12)(C9H7NO)(P(C6H5)3)](1+)*ClO4(1-)=[Rh(C8H12)(C9H7NO)(P(C6H5)3)]ClO4 (112312-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: triphenylphosphine / not given

With triphenylphosphine; In acetone;

DOI:10.1016/S0020-1693(00)81246-3

Reference yield:

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium (12092-47-6) → [Rh(C8H12)(C9H7NO)(P(C6H5)3)](1+)*ClO4(1-)=[Rh(C8H12)(C9H7NO)(P(C6H5)3)]ClO4 (112312-54-6)

Guidance literature:

Multi-step reaction with 2 steps

1: acetone

2: triphenylphosphine / not given

With triphenylphosphine; In acetone;

DOI:10.1016/S0020-1693(00)81246-3

upstream raw materials:

isoquinoline N-oxide

[Rh(C₈H₁₂)(C₉H₇NO)2]⁽¹⁺⁾*ClO₄^(1-)=[Rh(C₈H₁₂)(C₉H₇NO)2]ClO₄

isoquinoline-N-oxide hydrate

di-μ-chloro-bis(1,5-cyclooctadiene)dirhodium