Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2⁽¹⁺⁾*BF₄^(1-)=Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2BF₄

Base Information

Chemical Name:Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2⁽¹⁺⁾*BF₄^(1-)=Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2BF₄
CAS No.:90552-98-0
Molecular Formula:BF₄*C₅₂H₄₄ClIr₂O₂P₄
Molecular Weight:1331.51
Hs Code.:

Ir<sub>2</sub>Cl(CO)2(((C<sub>6</sub>H<sub>5</sub>)2P)2CH<sub>2</sub>)2<sup>(1+)</sup>*BF<sub>4</sub><sup>(1-)</sup>=Ir<sub>2</sub>Cl(CO)2(((C<sub>6</sub>H<sub>5</sub>)2P)2CH<sub>2</sub>)2BF<sub>4</sub>

Synonyms:Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2⁽¹⁺⁾*BF₄^(1-)=Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2BF₄

Suppliers and Price of Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2⁽¹⁺⁾*BF₄^(1-)=Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2BF₄

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2⁽¹⁺⁾*BF₄^(1-)=Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2BF₄

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2⁽¹⁺⁾*BF₄^(1-)=Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2BF₄

There total 2 articles about Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2⁽¹⁺⁾*BF₄^(1-)=Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2BF₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 503-17-3
dimethylacetylene

: 97690-07-8
{Ir2(H)2(CO)2(μ-Cl)(bis(diphenylphosphino)methane)2}{BF4}

: 106-98-9,9003-28-5
1-butylene

: 90552-98-0
{Ir2(CO)2(μ-Cl)(bis(diphenylphosphino)methane)2}{BF4}

Guidance literature:: In dichloromethane; byproducts: cis-butene, trans-butene; (N2); dry solvents; excess of 2-butyne; Ir-compd. not isolated, (1)H- and (31)P-NMR spectroscopic monitoring;

Reference yield:

: 97690-07-8
{Ir2(H)2(CO)2(μ-Cl)(bis(diphenylphosphino)methane)2}{BF4}

: 536-74-3
phenylacetylene

: 90552-98-0
{Ir2(CO)2(μ-Cl)(bis(diphenylphosphino)methane)2}{BF4}

Guidance literature:: In not given; byproducts: styrene; (N2); dry solvents; immediate appearance; not isolated, (1)H- and (31)P-NMR spectroscopic monitoring;

Reference yield: 90.0%

: 90552-98-0
Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2⁽¹⁺⁾*BF₄^(1-)=Ir₂Cl(CO)2(((C₆H₅)2P)2CH₂)2BF₄

: 97690-07-8
{Ir2(H)2(CO)2(μ-Cl)(bis(diphenylphosphino)methane)2}{BF4}

Guidance literature:: With H₂; In tetrahydrofuran; stirring as a slurry in THF under 1 atm of H2 for 15 min, solid diappearing to give a clear light yellow soln., H2 replacing to N2, refluxing for 20 min, taking to dryness under a stream of N2; purified by recrystallization from CH2Cl2-Et2O, identified by elem. anal., IR and NMR spectra;