deuterated vanillin

Base Information

Chemical Name:deuterated vanillin
CAS No.:92351-94-5
Molecular Formula:C₈H₈O₃
Molecular Weight:153.142
Hs Code.:

Synonyms:deuterated vanillin

Suppliers and Price of deuterated vanillin

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of deuterated vanillin

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of deuterated vanillin

There total 8 articles about deuterated vanillin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 109685-12-3
C₉H₁₁⁽²⁾HO₃

: 92351-94-5
deuterated vanillin

Guidance literature:: With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1016/S0040-4039(00)96778-9

Reference yield:

: 5533-03-9
2-methoxy-4-methoxymethylphenol

: 92351-94-5
deuterated vanillin

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi 2.) D₂O / 1.) THF, hexanes, r.t., 4 h 2.) THF, -40 deg C, 30 min then warming up to r.t. for 2 h

2: 90 percent / DDQ / CH₂Cl₂; H₂O

With n-butyllithium; water-d2; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In dichloromethane; water;
DOI:10.1016/S0040-4039(00)96778-9