4-sulfamoylphenylacetamide

Base Information

Chemical Name:4-sulfamoylphenylacetamide
CAS No.:1082068-60-7
Molecular Formula:C₈H₁₀N₂O₃S
Molecular Weight:214.245
Hs Code.:

Synonyms:4-sulfamoylphenylacetamide

Suppliers and Price of 4-sulfamoylphenylacetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of 4-sulfamoylphenylacetamide

Chemical Property:

Purity/Quality:

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Technology Process of 4-sulfamoylphenylacetamide

There total 5 articles about 4-sulfamoylphenylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

: 22958-99-2
2-(4-(chlorosulfonyl)phenyl)acetic acid

: 1082068-60-7
4-sulfamoylphenylacetamide

Guidance literature:: 2-(4-(chlorosulfonyl)phenyl)acetic acid; With thionyl chloride; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

With ammonia; In acetonitrile; at 0 - 20 ℃; for 3h;
DOI:10.5012/bkcs.2012.33.2.721

Reference yield:

: C₈H₆Cl₂O₃S

: 1082068-60-7
4-sulfamoylphenylacetamide

Guidance literature:: With ammonia; In acetonitrile; at 20 ℃;
DOI:10.1016/j.bmcl.2009.11.067

Reference yield:

: 103-82-2
phenylacetic acid

: 1082068-60-7
4-sulfamoylphenylacetamide

Guidance literature:: Multi-step reaction with 3 steps

1: chlorosulfonic acid / 24 h / 0 - 20 °C

2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 17 h / 20 °C

3: ammonia / acetonitrile / 24 h / 20 °C

With chlorosulfonic acid; oxalyl dichloride; ammonia; N,N-dimethyl-formamide; In dichloromethane; acetonitrile;
DOI:10.1016/j.bmcl.2014.02.074