(E)-1-(Dimethylphenylsilyl)-1-buten-3-ol ((tert-butyldimethylsilyl)oxy)acetate

Base Information

Chemical Name:(E)-1-(Dimethylphenylsilyl)-1-buten-3-ol ((tert-butyldimethylsilyl)oxy)acetate
CAS No.:133323-30-5
Molecular Formula:C₂₀H₃₄O₃Si₂
Molecular Weight:378.659
Hs Code.:

Synonyms:(E)-1-(Dimethylphenylsilyl)-1-buten-3-ol ((tert-butyldimethylsilyl)oxy)acetate

Suppliers and Price of (E)-1-(Dimethylphenylsilyl)-1-buten-3-ol ((tert-butyldimethylsilyl)oxy)acetate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (E)-1-(Dimethylphenylsilyl)-1-buten-3-ol ((tert-butyldimethylsilyl)oxy)acetate

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Technology Process of (E)-1-(Dimethylphenylsilyl)-1-buten-3-ol ((tert-butyldimethylsilyl)oxy)acetate

There total 1 articles about (E)-1-(Dimethylphenylsilyl)-1-buten-3-ol ((tert-butyldimethylsilyl)oxy)acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 137120-08-2
(E)-(±)-1-(dimethylphenylsilyl)-1-buten-3-ol

: 105459-05-0
{[tert-butyl(dimethyl)silyl]oxy}acetic acid

: 133323-30-5
(E)-1-(Dimethylphenylsilyl)-1-buten-3-ol ((tert-butyldimethylsilyl)oxy)acetate

Guidance literature:: With dicyclohexyl-carbodiimide; dmap; In dichloromethane; Ambient temperature;
DOI:10.1021/jo00010a046

Reference yield:

: 133323-30-5
(E)-1-(Dimethylphenylsilyl)-1-buten-3-ol ((tert-butyldimethylsilyl)oxy)acetate

: 133323-26-9,133323-27-0
(E)-(2S,3R)-2-((tert-Butyldiphenylsilyl)oxy)-3-(dimethylphenylsilyl)-4-hexenoic acid

: 133323-38-3,133323-39-4
(E)-(2R^*,3R^*)-2-((tert-Butyldimethylsilyl)oxy)-3-(dimethylphenylsilyl)-4-hexenoic acid

: 133323-38-3,133323-39-4
(E)-(2S^*,3R^*)-2-((tert-Butyldimethylsilyl)oxy)-3-(dimethylphenylsilyl)-4-hexenoic acid

Guidance literature:: With pyridine; chloro-trimethyl-silane; lithium diisopropyl amide; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts; 1.) THF, -78 deg C; 2.) -78 deg C to 0 deg C, 1 h;
DOI:10.1021/jo00010a046