1-[(1S)-(2-chlorophenyl){methyl[(1'S)-1'-phenylethyl]amino}methyl]-2-naphthol

Base Information

Chemical Name:1-[(1S)-(2-chlorophenyl){methyl[(1'S)-1'-phenylethyl]amino}methyl]-2-naphthol
CAS No.:1280211-25-7
Molecular Formula:C₂₆H₂₄ClNO
Molecular Weight:401.936
Hs Code.:

Synonyms:1-[(1S)-(2-chlorophenyl){methyl[(1'S)-1'-phenylethyl]amino}methyl]-2-naphthol

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Chemical Property of 1-[(1S)-(2-chlorophenyl){methyl[(1'S)-1'-phenylethyl]amino}methyl]-2-naphthol

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Technology Process of 1-[(1S)-(2-chlorophenyl){methyl[(1'S)-1'-phenylethyl]amino}methyl]-2-naphthol

There total 4 articles about 1-[(1S)-(2-chlorophenyl){methyl[(1'S)-1'-phenylethyl]amino}methyl]-2-naphthol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

: 1280211-48-4
C₂₆H₂₂ClNO

: 1280211-25-7
1-[(1S)-(2-chlorophenyl){methyl[(1'S)-1'-phenylethyl]amino}methyl]-2-naphthol

Guidance literature:: C₂₆H₂₂ClNO; With sodium tetrahydroborate; acetic acid; In tetrahydrofuran; at 0 - 20 ℃;

With sodium carbonate; In tetrahydrofuran; water; at 20 ℃;
DOI:10.1002/chir.20903

Reference yield:

: 2627-86-3
(S)-1-phenyl-ethylamine

: 1280211-25-7
1-[(1S)-(2-chlorophenyl){methyl[(1'S)-1'-phenylethyl]amino}methyl]-2-naphthol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 60 °C / Inert atmosphere

2.1: tetrahydrofuran; water / 15 h / 20 °C

3.1: sodium tetrahydroborate; acetic acid / tetrahydrofuran / 0 - 20 °C

3.2: 20 °C

With sodium tetrahydroborate; acetic acid; In tetrahydrofuran; water;
DOI:10.1002/chir.20903

Reference yield:

: 135-19-3
β-naphthol

: 1280211-25-7
1-[(1S)-(2-chlorophenyl){methyl[(1'S)-1'-phenylethyl]amino}methyl]-2-naphthol

Guidance literature:: Multi-step reaction with 3 steps

1.1: 60 °C / Inert atmosphere

2.1: tetrahydrofuran; water / 15 h / 20 °C

3.1: sodium tetrahydroborate; acetic acid / tetrahydrofuran / 0 - 20 °C

3.2: 20 °C

With sodium tetrahydroborate; acetic acid; In tetrahydrofuran; water;
DOI:10.1002/chir.20903