3-methyl-2-oxo-5-phenyl-1,4,6,9-tetraoxa-5-phosphaspiro<4.4>nonane

Base Information

• Chemical Name: 3-methyl-2-oxo-5-phenyl-1,4,6,9-tetraoxa-5-phosphaspiro<4.4>nonane
• CAS No.: 61356-99-8
• Molecular Formula: C₁₁H₁₃O₅P
• Molecular Weight: 256.195
• Mol file: 61356-99-8.mol

Synonyms:3-methyl-2-oxo-5-phenyl-1,4,6,9-tetraoxa-5-phosphaspiro<4.4>nonane

Chemical Property of 3-methyl-2-oxo-5-phenyl-1,4,6,9-tetraoxa-5-phosphaspiro<4.4>nonane

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-methyl-2-oxo-5-phenyl-1,4,6,9-tetraoxa-5-phosphaspiro<4.4>nonane

There total 2 articles about 3-methyl-2-oxo-5-phenyl-1,4,6,9-tetraoxa-5-phosphaspiro<4.4>nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

LACTIC ACID (849585-22-4,106989-11-1,26811-96-1,31587-11-8,26100-51-6) + 2-phenyl-[1,3,2]dioxaphospholane (1006-83-3) → 3-methyl-2-oxo-5-phenyl-1,4,6,9-tetraoxa-5-phosphaspiro<4.4>nonane (61356-99-8)

Guidance literature:

With diphenyldisulfane; In diethyl ether; at 0 ℃; for 3h;

DOI:10.1021/jo00345a003

Reference yield:

2-oxo-propionic acid (127-17-3) + 2-phenyl-[1,3,2]dioxaphospholane (1006-83-3) → 3-methyl-2-oxo-5-phenyl-1,4,6,9-tetraoxa-5-phosphaspiro<4.4>nonane (61356-99-8)

Guidance literature:

In diethyl ether;

DOI:10.1021/ja00440a075

upstream raw materials:

2-oxo-propionic acid

2-phenyl-[1,3,2]dioxaphospholane

LACTIC ACID