2--7-endo-acetylisoquinuclidene

Base Information

Chemical Name:2--7-endo-acetylisoquinuclidene
CAS No.:120230-11-7
Molecular Formula:C₂₅H₂₆N₂O₃S
Molecular Weight:434.559
Hs Code.:

2-<N-(phenylsulfonyl)tryptophyl>-7-endo-acetylisoquinuclidene

Synonyms:2--7-endo-acetylisoquinuclidene

Suppliers and Price of 2--7-endo-acetylisoquinuclidene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2--7-endo-acetylisoquinuclidene

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Technology Process of 2--7-endo-acetylisoquinuclidene

There total 3 articles about 2--7-endo-acetylisoquinuclidene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 120230-10-6
2--7-endo-<1,1-(ethylenedioxy)ethyl>isoquinuclidene

: 120230-11-7
2--7-endo-acetylisoquinuclidene

Guidance literature:: With sulfuric acid; silica gel; In dichloromethane; at 25 ℃; for 40h;
DOI:10.1021/jo00273a024

Reference yield:

: 87371-63-9,90693-43-9
(1S,4S,7R)-2-[2-(1H-Indol-3-yl)-ethyl]-7-(2-methyl-[1,3]dioxolan-2-yl)-2-aza-bicyclo[2.2.2]oct-5-ene

: 120230-11-7
2--7-endo-acetylisoquinuclidene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, from -78 deg C to 0 deg C, 0.5 h, 2.) THF, hexane, 25 deg C, 12 h

2: 94 percent / 10percent H₂SO₄, silica gel 60 / CH₂Cl₂ / 40 h / 25 °C

With n-butyllithium; sulfuric acid; silica gel; In dichloromethane;
DOI:10.1021/jo00273a024

Reference yield:

: 98-09-9
benzenesulfonyl chloride

: 120230-11-7
2--7-endo-acetylisoquinuclidene

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) n-BuLi / 1.) THF, hexane, from -78 deg C to 0 deg C, 0.5 h, 2.) THF, hexane, 25 deg C, 12 h

2: 94 percent / 10percent H₂SO₄, silica gel 60 / CH₂Cl₂ / 40 h / 25 °C

With n-butyllithium; sulfuric acid; silica gel; In dichloromethane;
DOI:10.1021/jo00273a024